一种新型香蕉形化合物的酯化设计与合成

Diyala Journal for Pure Science Pub Date : 2021-10-01 DOI:10.24237/djps.17.04.568c

Omar Mahdi, H. K. Salih, A. Kshash

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引用次数: 0

摘要

以对氨基苯甲酸和烷氧苯甲醛为原料，在无水乙醇中合成希夫碱，并以DCC (N,N'-二环碳二亚胺)和DAMP(4-(二甲氨基)吡啶为原料，与(E)-3-((E)-4-((E)-4-((E)-4-烷氧基苄基)氨基苯甲酸酯反应生成3-((E)-4-((E)-4-烷氧基苄基)氨基苯甲酸酯。产物的熔点、FT-IR、1HNMR谱图证实了产物的结构。

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Design, Synthesis of a Novel Banana-Shaped Compounds via Esterification

Schiff's Bases were synthesized from the reaction of p-amino benzoic acid and alkoxybenzaldehyde in absolute ethanol and reacted with (E)-3-((4-hydroxybenzylidene) amino) phenol used DCC (N,N'-Dicyclocarbodiimide) and DAMP (4-(Dimethylamino) pyridine ) to 3-(((E)-4-((4-(((E)-4 alkoxy benzylidene) amino) benzoyl) oxy) benzylidene) amino) phenyl4- (E)- 4-alkoxy benzyli dene ) amino) benzoate. The structures of the products were confirmed by their melting points, FT-IR, 1HNMR spectra.

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Diyala Journal for Pure Science

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