微波辅助合成混合金属氧化物纳米颗粒

Journal of Nanoparticles Pub Date : 2013-03-20 DOI:10.1155/2013/737831

A. Verma, R. Dwivedi, R. Prasad, K. S. Bartwal

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引用次数: 26

摘要

采用微波辅助柠檬酸溶胶-凝胶法和溶液燃烧法制备了ZrO2、ZrTiO4和ZrV2O7混合金属氧化物纳米颗粒。利用XRD和TEM技术对制备的纳米颗粒进行了结构表征。拉曼谱带的展宽是由于Zr4的随机分布所引起的局部成分波动或局部位置无序造成的

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Microwave-Assisted Synthesis of Mixed Metal-Oxide Nanoparticles

Nanoparticles of mixed metal oxides, ZrO2, ZrTiO4, and ZrV2O7 were prepared by microwave-assisted citrate sol-gel and solution combustion method. The prepared nanoparticles were characterized for their structural details using XRD and TEM techniques. The broadening of Raman bands is ascribed to local compositional fluctuations or local positional disordering produced due to random distribution of Zr4

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Journal of Nanoparticles

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