慢蒸发法制备丝氨酸醋酸锌有机非线性光学材料的合成、晶体生长及表征

R. Sakunthaladevi
{"title":"慢蒸发法制备丝氨酸醋酸锌有机非线性光学材料的合成、晶体生长及表征","authors":"R. Sakunthaladevi","doi":"10.5185/amp.2019.0020","DOIUrl":null,"url":null,"abstract":"Optically good quality single crystal of Serine Zinc Acetate (SZA) was grown by the method of slow evaporation and using a solvent of water. The value of cell parameters was obtained by single crystal XRD study. The various functional groups of molecules present in SZA were identified from FTIR studies. The optical behaviour of the grown crystal was analysed through UV-VIS-NIR spectral studies and the material SZA was found to have wide range of transparency in the visible region. The Vickers micro hardness study revealed the hardening nature of the grown material. Thermal stability of SZA was confirmed using thermo gravimetric and differential thermal analyses. The NLO activity of the grown crystal was tested by Kurtz-Perry powder technique. Copyright © VBRI Press.","PeriodicalId":7297,"journal":{"name":"Advanced Materials Proceedings","volume":"34 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2019-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis, Crystal Growth and Characterization of Serine Zinc Acetate an Organic Nonlinear Optical material by Slow Evaporation Method\",\"authors\":\"R. Sakunthaladevi\",\"doi\":\"10.5185/amp.2019.0020\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Optically good quality single crystal of Serine Zinc Acetate (SZA) was grown by the method of slow evaporation and using a solvent of water. The value of cell parameters was obtained by single crystal XRD study. The various functional groups of molecules present in SZA were identified from FTIR studies. The optical behaviour of the grown crystal was analysed through UV-VIS-NIR spectral studies and the material SZA was found to have wide range of transparency in the visible region. The Vickers micro hardness study revealed the hardening nature of the grown material. Thermal stability of SZA was confirmed using thermo gravimetric and differential thermal analyses. The NLO activity of the grown crystal was tested by Kurtz-Perry powder technique. Copyright © VBRI Press.\",\"PeriodicalId\":7297,\"journal\":{\"name\":\"Advanced Materials Proceedings\",\"volume\":\"34 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2019-09-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Advanced Materials Proceedings\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.5185/amp.2019.0020\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Advanced Materials Proceedings","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.5185/amp.2019.0020","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

以水为溶剂,采用缓慢蒸发法制备了光学性能优良的丝氨酸醋酸锌单晶。通过单晶XRD研究得到了电池参数的取值。通过FTIR研究确定了SZA中存在的各种功能基团。通过紫外-可见-近红外光谱研究分析了生长晶体的光学行为,发现材料SZA在可见光区域具有广泛的透明度。维氏显微硬度研究揭示了生长材料的硬化性质。热重分析和差热分析证实了SZA的热稳定性。采用Kurtz-Perry粉末法测定了生长晶体的NLO活性。版权所有©VBRI出版社。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis, Crystal Growth and Characterization of Serine Zinc Acetate an Organic Nonlinear Optical material by Slow Evaporation Method
Optically good quality single crystal of Serine Zinc Acetate (SZA) was grown by the method of slow evaporation and using a solvent of water. The value of cell parameters was obtained by single crystal XRD study. The various functional groups of molecules present in SZA were identified from FTIR studies. The optical behaviour of the grown crystal was analysed through UV-VIS-NIR spectral studies and the material SZA was found to have wide range of transparency in the visible region. The Vickers micro hardness study revealed the hardening nature of the grown material. Thermal stability of SZA was confirmed using thermo gravimetric and differential thermal analyses. The NLO activity of the grown crystal was tested by Kurtz-Perry powder technique. Copyright © VBRI Press.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信