溶胶-凝胶法制备氧化锌纳米颗粒,研究其结构、光学性质和形貌

M. Junaid
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摘要

氧化锌纳米颗粒以其独特的特性和在光电器件中的应用,被归类为一种多用途材料。本研究着眼于氧化锌纳米粒子的形态、结构和光学特征。采用溶胶-凝胶法制备了以硝酸锌[Zn (NO3)2.4H2O]和氢氧化钠[NaOH]为前驱体的氧化锌纳米颗粒。主要目的是利用溶胶-凝胶法合成氧化锌纳米颗粒,因为这种方法易于实现,并且可以通过系统地监测反应条件来调节颗粒大小和形态。利用x射线衍射现象、扫描电子显微镜和紫外可见光谱表征技术来确定所制备的氧化锌纳米颗粒的结构、形态和光学特征。XRD检测表明,制备的纳米颗粒具有高结晶性。在所有衍射峰中观察到ZnO的高结晶度,表明采用溶胶-凝胶法制备了氧化锌纳米颗粒。由于ZnO纳米粒子的存在,紫外可见光谱在370nm处产生了吸收光谱。扫描电子显微镜(SEM)测量揭示了不同分辨率下氧化锌纳米颗粒的表面结构和晶粒尺寸。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis of Zinc Oxide Nanoparticles by Sol-gel method to Study its Structural Optical Properties and Morphology
Zinc oxide nanoparticles can be classified as a multipurpose material, along with their distinctive features and applications in optoelectronic devices. This research looks at the morphological, structural, and optical features of zinc oxide (ZnO) nanoparticles. The sol-gel procedure has been used to form zinc oxide nanoparticles with zinc nitrate [Zn (NO3)2.4H2O] and sodium hydroxide [NaOH] as precursors. The main objective is to synthesize zinc oxide (ZnO) nanoparticles by using the sol-gel approach because that is easy to implement and offers the capacity to adjust particle size and morphology by systematically monitoring reaction conditions. X-ray diffraction phenomenon, Scanning Electron Microscopy, and Ultraviolet-vis spectroscopy characterization techniques were used to determine the structural, morphological, and optical features of produced zinc oxide nanoparticles. According to the XRD examination, the produced nanoparticles are in a highly crystalline phase nature. The high crystallinity of ZnO is observed in all diffraction peaks, implying that Zinc oxide nanoparticles were synthesized properly using the sol-gel process. The UV-vis spectroscopy produced an absorption spectrum at 370nm due to ZnO nanoparticles. The Scanning Electron Microscopy (SEM) measurements reveal the surface structure and grains size of zinc oxide (ZnO) nanoparticles at a different resolution.
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