荧光光谱法测定润滑油耗度(DoC)

Rawnaq Qahtan Abdul Kareem, K. Al-Janabi
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引用次数: 0

摘要

提出了一种快速、廉价、简便的判别不同种类油脂及其功效的方法“消费度”(DoC)。荧光光谱法为油品检测提供了一种可靠的方法,无需繁琐的分离。调查了伊拉克当地市场上不同的新旧油样。而挑战是建立一个目录,其中包含所有在当地市场上可用的油的数据。该方法旨在控制伪造(伪造)商标的机油和区分不同的油。测定了油样在200 ~ 600 nm范围内的激发发射光谱。通过在稀释后的油液中加入几毫克的(Cu, Al, Fe)来考虑微量金属的存在对油液荧光强度的影响。对荧光强度没有明显影响。研究建议在车辆上安装一个简单的荧光光谱仪,定期检查机油的DoC,并准确地通知司机何时更换机油。试验结果表明,将该装置安装在汽车上,对发动机油质量和油耗进行常规检测是可行的。同时也证明了该技术在石油识别方面的潜力,并可以进一步发展。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Determination of the Degree of Consumption (DoC) of Lube Engine Oils Using Fluorescence Spectroscopy
The accreditation of a fast, inexpensive, and simple way to discriminate between different kinds of oils and their efficacy “degree of consumption (DoC)” has been developed. The fluorescence spectroscopy provides a reliable method for oil inspection without resorting to tedious separation. Different new and used oil samples available in the local Iraqi market were investigated. While the challenge is to build a directory containing data of all the oils available in the local market. This method expected to control the falsified (forged) trademarks of motor oils and to discriminate between different oils. The excitation-emission spectra of oil samples were determined in the range of 200 – 600 nm. The effect of the presence of trace metals on the fluorescence intensity of oils was considered by adding few milligrams of (Cu, Al, Fe) to the diluted oil solution. No major effect noticed on fluorescence intensity. The research suggests installing a simple Spectrofluorometer into vehicles to check the DoC of the oil regularly and to notify the driver exactly when to replace the engine oil. The obtained results indicate the applicability to execute such gadget to be installed in the vehicles for routine detection of the engine oil quality and its degree of consumption DoC. As well as demonstrate the potential of the technique in oil identification and could be further developed.
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