氢化物发生原子荧光光谱法测定口红中总砷

M. E. Ghanjaoui, I. Adraoui, A. Gammoun, L. Cervera, M. El Rhazi, M. de la Guardia
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引用次数: 0

摘要

本研究旨在确定口红中砷的总浓度,并评估每日从该产品中摄入这种有毒元素所带来的潜在健康风险。矿化和氢化物生成后,采用原子荧光光谱法(HG-AFS)对样品进行分析。在0.125 ~ 2µg L-1的浓度范围内,校正曲线呈线性,回归系数为0.9899数量级。检测限为3 ng g-1。标准差约为4%。通过计算三种口红样品中砷的添加回收率,评价了该方法的准确性。结果表明,回收率在91% ~ 98%之间。结果表明,本方法适用于口红样品中砷的检测。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Hydride generation atomic fluorescence spectrometry (HG-AFS) determination of total arsenic in lipstick
This study aimed to determine the total arsenic concentration in lipsticks and evaluate the potential health risks due to daily ingestion of this toxic element from this product. The samples were analyzed using atomic fluorescence spectrometry technique after mineralization and hydride generation (HG-AFS). The calibration curve is linear over a concentration range from 0.125 to 2 µg L-1 with a regression coefficient of the order of 0.9899. The limit of detection is reaches 3 ng g-1. The standard deviation is of the order of 4%.The accuracy of this method was evaluated by calculating the recoveries of additions of arsenic to three lipstick samples. These results indicate recovery rates between 91% and 98%. Finely, the results found demonstrate that the method used in this work is suitable for arsenic detection in lipsticks samples.  
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