利用榕叶水提物制备吸附有机染料的纳米磁铁矿

A. Ramesh, B. Lavakusa, B. Mohan, Y. P. Kumar, D. Devi, K. Basavaiah
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引用次数: 7

摘要

采用紫外可见光谱(UV-Vis)、傅里叶变换红外光谱(FTIR)、粉末x射线衍射(XRD)、场发射扫描电子显微镜(FESEM)、红外光谱(FTIR)等对合成的Fe3O4纳米粒子的光学形貌、晶体形貌、结构形貌和磁性行为进行了表征。透射电子显微镜(TEM)和振动样品磁强计(VSM)。吸收光谱在379 nm处出现峰值,证实了Fe3O4 NPs的形成。XRD结果表明,制备的Fe3O4 NPs具有立方反尖晶石结构,晶粒尺寸为11.04 nm。FESEM和TEM图像清楚地表明,Fe3O4纳米粒子呈球形,平均粒径为10.96 nm。电子衍射(SAED)图中选择区域的明亮圆形圆环显示出良好的结晶度。VSM结果显示Fe3O4 NPs具有超顺磁性。合成的Fe3O4 NPs具有吸附亚甲基蓝(MB)的潜力。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
A Facile Plant Mediated Synthesis of Magnetite Nanoparticles Using Aqueous Leaf Extract of Ficus Hispida L. for Adsorption of Organic Dye
A facile and eco-friendly method for the synthesis of magnetite nanoparticles (Fe3O4 NPs) via CoPrecipitation in the presence of aqueous leaf extract of Ficus hispida L. The optical, crystalline, structural morphology and magnetic behaviour of the synthesized Fe3O4 NPs were characterized by Ultraviolet-Visible (UV-Vis), Fourier transform infrared (FTIR) spectroscopy, powder X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), and transmission electron microscopy (TEM) and vibrating sample magnetometer (VSM). The absorption spectrum reveals the peak at 379 nm, which confirm the formations of Fe3O4 NPs. XRD results reveals the formation of phase pure Fe3O4 NPs with cubic inverse spinel structure with crystallite sizes of 11.04 nm. The FESEM and TEM images clearly show that the spherical shape of Fe3O4 NPs with average particles size of 10.96 nm. Bright circular rings in the selected area electron diffraction (SAED) pattern showed good crystallinity. VSM results show super paramagnetic behaviour of Fe3O4 NPs. The synthesized Fe3O4 NPs have potential to adsorption of Methylene Blue(MB)
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