A. Dandia, Ruby Singh, C. Mérienne, G. Morgant, A. Loupy
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引用次数: 11
摘要
报道了一种改进的微波辐射下一锅快速合成3 ' -(氟苯基)-螺[3h -吲哚-3,2 ' -四氢-1,3-噻嗪]-2,4 ' (1H)-二酮的方法。所报道的化合物的晶体结构已由x射线衍射测定。分子主要是平面,晶胞参数= 11.181 (9),b = 11.06 (1) a, c = 12.715(12),α= 90°,β= 98.31(7)°,γ= 90°。
Solvent-free one-pot synthesis and crystal structure of a spiro[indole-thiazine]
An improved facile one-pot synthesis of 3′-(fluorophenyl)-spiro[3H-indole-3,2′-tetrahydro-1,3-thiazine]-2,4′(1H)-dione is reported using an environmentally friendly green chemistry procedure under microwave irradiation. The crystal structure of the reported compound has been determined by a X-ray diffraction. The molecule is largely planar and has cell parameters of a = 11.181(9) Å, b = 11.06(1) Å, c = 12.715(12) Å, α = 90°, β = 98.31(7)°, γ = 90°.
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