微波辅助合成3′，3-苄基-双-4-羟基香豆素及其晶体结构

2009 Symposium on Photonics and Optoelectronics Pub Date : 2009-09-01 DOI:10.1109/SOPO.2009.5230279

Sheying Dong, Penghui Zhang, Jing Li

{"title":"微波辅助合成3′，3-苄基-双-4-羟基香豆素及其晶体结构","authors":"Sheying Dong, Penghui Zhang, Jing Li","doi":"10.1109/SOPO.2009.5230279","DOIUrl":null,"url":null,"abstract":"benzylidene-bis-4-hydroxycoumarin(BBHC) was prepared by using a microwave synthetic route in which 4- hydroxycoumarin was treated with benzaldehyde in the presence of ethanol. The formation of BBHC was characterized by IR, 1 H-NMR, MS and elemental analysis. Its crystal structure was determined by X-ray single crystal diffraction. Compared with BBHC synthesized by conventional heating methods, there was no isomerism phenomenon in their structures.","PeriodicalId":6416,"journal":{"name":"2009 Symposium on Photonics and Optoelectronics","volume":"9 1","pages":"1-2"},"PeriodicalIF":0.0000,"publicationDate":"2009-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Microwave-Assisted Synthesis and Crystal Structure of 3',3-Benzylidene-Bis-4-Hydroxycoumarin\",\"authors\":\"Sheying Dong, Penghui Zhang, Jing Li\",\"doi\":\"10.1109/SOPO.2009.5230279\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"benzylidene-bis-4-hydroxycoumarin(BBHC) was prepared by using a microwave synthetic route in which 4- hydroxycoumarin was treated with benzaldehyde in the presence of ethanol. The formation of BBHC was characterized by IR, 1 H-NMR, MS and elemental analysis. Its crystal structure was determined by X-ray single crystal diffraction. Compared with BBHC synthesized by conventional heating methods, there was no isomerism phenomenon in their structures.\",\"PeriodicalId\":6416,\"journal\":{\"name\":\"2009 Symposium on Photonics and Optoelectronics\",\"volume\":\"9 1\",\"pages\":\"1-2\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2009-09-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"2009 Symposium on Photonics and Optoelectronics\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1109/SOPO.2009.5230279\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"2009 Symposium on Photonics and Optoelectronics","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/SOPO.2009.5230279","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}

引用次数: 0

摘要

以4-羟基香豆素为原料，在乙醇存在下用苯甲醛处理，采用微波合成方法制备了苄基双-4-羟基香豆素(BBHC)。采用IR、1h - nmr、MS和元素分析对BBHC的形成进行了表征。用x射线单晶衍射测定了其晶体结构。与传统加热方法合成的BBHC相比，其结构中没有异构现象。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

查看原文本刊更多论文

Microwave-Assisted Synthesis and Crystal Structure of 3',3-Benzylidene-Bis-4-Hydroxycoumarin

benzylidene-bis-4-hydroxycoumarin(BBHC) was prepared by using a microwave synthetic route in which 4- hydroxycoumarin was treated with benzaldehyde in the presence of ethanol. The formation of BBHC was characterized by IR, 1 H-NMR, MS and elemental analysis. Its crystal structure was determined by X-ray single crystal diffraction. Compared with BBHC synthesized by conventional heating methods, there was no isomerism phenomenon in their structures.

求助全文

通过发布文献求助，成功后即可免费获取论文全文。去求助

来源期刊

2009 Symposium on Photonics and Optoelectronics

自引率

0.00%

发文量