用LC-MS/MS定量分析唾液中七种类固醇

Journal of Applied Bioanalysis Pub Date : 2019-04-15 DOI:10.17145/JAB.19.006

E. Jurgens, EJ Knaven, N. Zheng, EC Hegeman, MW van Gemert, JM Emmen, I Willemen, Y. Mulder, L Ijsselstijn, B. D. Rooij, TH Noij

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引用次数: 3

摘要

表S1。所研究的潜在干扰的观测结果。名称[M+H]+ (M /z)保留时间(min.)潜在干扰测试保留时间差11α-羟孕酮331.2 17α-羟孕酮11β-羟孕酮331.2 10.50 17α-羟孕酮1.10 21-羟孕酮331.2 10.16 17α-羟孕酮1.44 β-雌二醇-6-酮287.2雄烯二酮醛固酮361.2 4.94可的松0.86皮质酮347.2 7.31 21-脱氧皮质醇0.00 11-脱氧皮质醇0.29脱氢表雄酮289.2睾酮表雄酮289.211.30睾酮1.90雌三醇289.2睾酮非诺贝特361.8可的松强的松361.2 5.57可的松0.23 =表明在目前的方法中对该成分的分析没有产生反应。

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Quantitative Profiling of Seven Steroids in Saliva using LC-MS/MS

Table S1. Obervations for the investigated potential interferences. Name [M+H]+ (m/z) Retention time (min.) Potentially interference tested for Retention time difference 11α-hydroxyprogesterone 331.2 17α-hydroxyprogesterone 11β-hydroxyprogesterone 331.2 10.50 17α-hydroxyprogesterone 1.10 21-hydroxyprogesterone 331.2 10.16 17α-hydroxyprogesterone 1.44 β-estradiol-6-one 287.2 Androstenedione Aldosterone 361.2 4.94 Cortisone 0.86 Corticosterone 347.2 7.31 21-deoxycortisol 0.00 11-deoxycortisol 0.29 Dehydroepiandrosterone 289.2 Testosterone Epitestosterone 289.2 11.30 Testosterone 1.90 Estriol 289.2 Testosterone Fenofibrate 361.8 Cortisone Prednisolone 361.2 5.57 Cortisone 0.23 = indicates that the analysis of that component did not result in a response in the current method.

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来源期刊

Journal of Applied Bioanalysis

CiteScore

1.00

自引率

0.00%

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