{"title":"药物的红外分析。1. 溴化钾圆盘技术在类固醇、生物碱、巴比妥酸盐等药物中的应用。","authors":"A. L. Hayden, O. R. Sammul","doi":"10.1002/JPS.3030490802","DOIUrl":null,"url":null,"abstract":"The quantitative potassium bromide disk technique has been investigated and methods have been adopted for its application to some pharmaceuticals. Average deviations from linearity within ±4.0 per cent were obtained with some crystalline compounds. Analyses of pharmaceutical preparations, by hand-grinding or vibrator-grinding methods, resulted in average agreement within ±3 to ±4.5 per cent with ultraviolet spectrophotometric or gravimetric determinations.","PeriodicalId":17210,"journal":{"name":"Journal of the American Pharmaceutical Association. American Pharmaceutical Association","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"1960-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"5","resultStr":"{\"title\":\"Infrared analysis of pharmaceuticals. 1. Application of the potassium bromide disk technique to some steroids, alkaloids, barbiturates, and other drugs.\",\"authors\":\"A. L. Hayden, O. R. Sammul\",\"doi\":\"10.1002/JPS.3030490802\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The quantitative potassium bromide disk technique has been investigated and methods have been adopted for its application to some pharmaceuticals. Average deviations from linearity within ±4.0 per cent were obtained with some crystalline compounds. Analyses of pharmaceutical preparations, by hand-grinding or vibrator-grinding methods, resulted in average agreement within ±3 to ±4.5 per cent with ultraviolet spectrophotometric or gravimetric determinations.\",\"PeriodicalId\":17210,\"journal\":{\"name\":\"Journal of the American Pharmaceutical Association. American Pharmaceutical Association\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1960-08-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"5\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of the American Pharmaceutical Association. American Pharmaceutical Association\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1002/JPS.3030490802\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of the American Pharmaceutical Association. American Pharmaceutical Association","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1002/JPS.3030490802","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Infrared analysis of pharmaceuticals. 1. Application of the potassium bromide disk technique to some steroids, alkaloids, barbiturates, and other drugs.
The quantitative potassium bromide disk technique has been investigated and methods have been adopted for its application to some pharmaceuticals. Average deviations from linearity within ±4.0 per cent were obtained with some crystalline compounds. Analyses of pharmaceutical preparations, by hand-grinding or vibrator-grinding methods, resulted in average agreement within ±3 to ±4.5 per cent with ultraviolet spectrophotometric or gravimetric determinations.
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