新型四唑-5-噻唑类三足配体的合成与结构

Journal of the Belarusian State University. Chemistry Pub Date : 2022-08-24 DOI:10.33581/2520-257x-2022-2-10-18

S. Voitekhovich, M. M. Degtyarik, A. Lyakhov, L. Ivashkevich, Yuri V. Grigoriev, O. Ivashkevich

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引用次数: 0

摘要

以1- r -四唑-5-噻唑为原料，与碘仿在碱性介质中烷基化，合成了R1 = Me, Ph的新型三脚配体(R1N4CS)3CH。根据单晶的元素分析、核磁共振光谱、热分析和x射线衍射分析等数据对这些配体进行了鉴定。

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Synthesis and structure of novel tripodal ligands based on tetrazol-5-thioles

Novel tripodal ligands (R1N4CS)3CH, where R1 = Me, Ph, were synthesised by alkylation of 1-R-tetrazol-5-thioles with iodoform in alkaline media. These ligands were identified based on data of elemental analysis, nuclear magnetic resonance spectroscopy, thermal analysis, and X-ray diffraction analysis of single crystals.

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Journal of the Belarusian State University. Chemistry

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