{"title":"异核(Co-Sr) 2,3-吡啶二羧酸配合物作为缺氧钙钛矿SrCoO2.52的前体","authors":"A. Lazarescu, E. Melnic, V. Kravtsov, C. Turta","doi":"10.1109/OMEE.2012.6464758","DOIUrl":null,"url":null,"abstract":"The heterometallic, single-source precursor with formula {[CoSr(2,3-pdc)<inf>2</inf>(H<inf>2</inf>O)<inf>5</inf>]·3H<inf>2</inf>O}<inf>n</inf> (1), has been synthesized and investigated by elemental analysis, IR-spectroscopy, thermal analysis (TGA) and single crystal X-ray diffraction. The compound 1 crystallizes in the triclinic space group P−1 and is self-organized in a polymeric structure of 2D dimension. Thermal decomposition of 1 leads to the formation of oxygen-deficient perovskite SrCoO<inf>2.52</inf>, as is determined by powder X-ray diffraction.","PeriodicalId":6332,"journal":{"name":"2012 IEEE International Conference on Oxide Materials for Electronic Engineering (OMEE)","volume":"7 1","pages":"299-300"},"PeriodicalIF":0.0000,"publicationDate":"2012-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Heteronuclear (Co-Sr) 2,3-pyridinedicarboxylate complex as precursor to the oxygen-deficient perovskite SrCoO2.52\",\"authors\":\"A. Lazarescu, E. Melnic, V. Kravtsov, C. Turta\",\"doi\":\"10.1109/OMEE.2012.6464758\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The heterometallic, single-source precursor with formula {[CoSr(2,3-pdc)<inf>2</inf>(H<inf>2</inf>O)<inf>5</inf>]·3H<inf>2</inf>O}<inf>n</inf> (1), has been synthesized and investigated by elemental analysis, IR-spectroscopy, thermal analysis (TGA) and single crystal X-ray diffraction. The compound 1 crystallizes in the triclinic space group P−1 and is self-organized in a polymeric structure of 2D dimension. Thermal decomposition of 1 leads to the formation of oxygen-deficient perovskite SrCoO<inf>2.52</inf>, as is determined by powder X-ray diffraction.\",\"PeriodicalId\":6332,\"journal\":{\"name\":\"2012 IEEE International Conference on Oxide Materials for Electronic Engineering (OMEE)\",\"volume\":\"7 1\",\"pages\":\"299-300\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2012-09-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"2012 IEEE International Conference on Oxide Materials for Electronic Engineering (OMEE)\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1109/OMEE.2012.6464758\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"2012 IEEE International Conference on Oxide Materials for Electronic Engineering (OMEE)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/OMEE.2012.6464758","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Heteronuclear (Co-Sr) 2,3-pyridinedicarboxylate complex as precursor to the oxygen-deficient perovskite SrCoO2.52
The heterometallic, single-source precursor with formula {[CoSr(2,3-pdc)2(H2O)5]·3H2O}n (1), has been synthesized and investigated by elemental analysis, IR-spectroscopy, thermal analysis (TGA) and single crystal X-ray diffraction. The compound 1 crystallizes in the triclinic space group P−1 and is self-organized in a polymeric structure of 2D dimension. Thermal decomposition of 1 leads to the formation of oxygen-deficient perovskite SrCoO2.52, as is determined by powder X-ray diffraction.
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