酸-胺偶联的工艺优化:催化方法

Q2 Chemistry

Current Chemistry Letters Pub Date : 2023-01-01 DOI:10.5267/j.ccl.2022.8.010

Ranjit C. Dabhi, Unnati Patel, Vaibhavi B. Rathod, Siddharth Shah, Jayesh J. Maru

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引用次数: 3

摘要

设计了不同芳香/脂肪酸与胺偶联形成酰胺键的有效途径。在优化后的反应条件下，转化率最高，不产生任何副产物。所有合成的化合物均采用柱层析纯化，并用质谱、核磁共振谱和液相色谱-质谱分析对其进行了表征。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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Process optimization for acid-amine coupling: a catalytic approach

Proficient routes were devised for coupling different aromatic/aliphatic acids with amines to form amide linkage using various catalysts. Under the optimized reaction conditions, highest conversion was possible without formation of any by-products. All synthesized compounds were purified using column chromatography and characterized by mass spectrometry, nuclear magnetic resonance spectrometry and liquid chromatography-mass spectrometric analysis.

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来源期刊

Current Chemistry Letters Chemistry-Chemistry (all)

CiteScore

4.90

自引率

0.00%

发文量

审稿时长

20 weeks

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