当地植物玫瑰花萼染料的酸碱指示剂性能

Onuegbu Genevieve, Nnorom Onyekachi, Okonkwo Samuel Nonso, Ojiaku Pascal
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引用次数: 0

摘要

从芙蓉花萼中提取染料,并将其作为酸碱指示剂,用于酸的标准化和部分选定酸的摩尔质量测定。花萼芙蓉去皮,洗净,在60°C的烤箱中加热。它被磨成粉末,浸泡在热乙醇和冷乙醇中提取。部分提取液经过滤后缓慢加热浓缩,得到1.5 kg的芙蓉指示剂。以0.03 M的碱浓度为基准,采用芙蓉的热萃取液和冷萃取液进行酸标准。在碱性培养基上进行的初步试验中,芙蓉花萼指示剂在酸性条件下呈红色,在碱性培养基中呈绿色,在滴定过程的终点,冷热指示剂都呈现出鲜明而强烈的颜色。然而,弱酸和弱碱(H2C2O4/Na2CO3和H2C2O4/B4Na2O7)没有颜色变化。测定了所用酸的平均体积,并用于测定研究工作中所用酸的摩尔浓度和质量浓度。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Acid-Base Indicator Properties of Dye from Local Plant: The Rosella Calyces (Hibiscus Sabdariffa)
The dye from the Calyces Hibiscus Sabdariffa (Zobo) was extracted and used as acid-base indicator for the standardization of acid and determination of the molar masses of some selected acids. The Calyces Hibiscus sabdariffa was peeled, washed and heated in an oven at 60°C. It was ground into powder and soaked in hot and cold ethanol for the extraction. Part of the extract was filtered and concentrated by subjecting the extract to slow heating which yielded 1.5 kg of the Hibiscus sabdariffa indicator. Hot and cold extracts of the Hibiscus sabdariffa were used for the standardization of acid with 0.03 M concentration of the bases. On the preliminary test carried out on basic medium, the calyces Hibiscus sabdariffa indicator turned red in acidic condition and green in basic medium, both hot and cold indicators yielded sharp and intense colours at the end points during titration processes. However, there were no colour changes for weak acid versus weak bases (H2C2O4/Na2CO3 and H2C2O4/B4Na2O7). The mean volumes of the acids used were determined and used for the determination of the molar concentration and mass concentration of all the acids used in the research work.
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