基于土耳其斯坦天然粘土的磁性复合材料MnFe2O4/粘土的合成与表征

Zh.A. Baimuratova, M. Kalmakhanova, B. Massalimova, A. Nurlibaeva, A.S. Kulazhanova, J. L. Diaz de Tuesta, H. Gomes
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引用次数: 0

摘要

本工作致力于开发一种在天然粘土上合成基于铁氧体锰磁性复合材料的新方法,并结合其物理化学特性。在研究中,从土耳其斯坦矿床获得的哈萨克斯坦天然粘土用于制备磁性复合材料。由于磁控材料在生物医学系统、电子器件、催化和吸附过程中的各种应用需要,形成具有磁性质的材料是我们这个时代的一项紧迫任务。这种材料的优点是能够使用磁场控制它们进行震动、回收、感应加热等。在这项工作中,锰和铁盐与5 mol L-1 NaOH在Turkestan粘土(TC)上共沉淀制备样品。通过傅里叶变换红外光谱(FTIR)、x射线衍射分析(XRD)和元素分析等方法对材料进行了表征。根据XRD和热分析的理化研究结果,高岭石是TC组成中的主要矿物。采用化学共沉淀法成功制备了具有良好磁选性能的磁性吸附剂MnFe2O4/粘土
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and characterization of a new magnetic composite MnFe2O4/clay based on a natural clay obtained from Turkestan deposit
The work is devoted to the development of a new method for the synthesis of magnetic composites based on manganese ferrite on a natural clay, coupling with their physico-chemical characterization. In the study, a natural clay of Kazakhstan obtained from the Turkestan deposit was used for the preparation of magnetic composites. The formation of materials with magnetic properties is an urgent task of our time, due to the needs of various applications of magnetically controlled materials for biomedical systems, electronic devices, catalytic and adsorption processes. The advantage of such materials is the ability to control them using a magnetic field for shaking, recovery, induction heating, among others. In this work, samples were prepared by co-precipitation of manganese and iron salts with 5 mol L-1 NaOH over the Turkestan clay (TC). Materials were characterized by various analyses, such as Fourier-Transform infrared spectroscopy (FTIR), X-ray diffractometric analysis (XRD), and elemental analysis. According to the results of physical and chemical studies of the XRD and thermal analysis, kaolinite is the main mineral in the composition of TC. Magnetic adsorbents MnFe2O4/clay with perfect magnetic separation characteristics were successfully obtained by chemical co-precipitation
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