核磁共振13C谱的一种现成的赋值方法:冰片13C谱的完整赋值

Journal of The Chemical Society D: Chemical Communications Pub Date : 1971-01-01 DOI:10.1039/C29710000364

J. Briggs, F. A. Hart, G. P. Moss, E. W. Randall

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引用次数: 23

摘要

用三-(2,2,6,6-四甲基庚二酮)镨Pr(tmhd)在龙脑13C nmr谱中引起顺磁位移;这些位移以及相应的铕和铽配合物引起的位移与根据它们的起源为伪接触性质计算的值吻合得很好。

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A ready method of assignment for 13C nuclear magnetic resonance spectra: the complete assignment of the 13C spectrum of borneol

Paramagnetic shifts induced in the 13C n.m.r. spectrum of borneol by tris-(2,2,6,6-tetramethylheptanedionato)praseodymium, Pr(tmhd), have been used in a total assignment; these shifts and those induced by the corresponding europium and terbium complexes agree well with values calculated on the basis that their origin is of a pseudo-contact nature.

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Journal of The Chemical Society D: Chemical Communications

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