绿色制备掺杂银钛酸盐的抗菌活性

A. C. Ha, T. Nguyen, P. Nguyen, V. M. Nguyen
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引用次数: 1

摘要

目标。本研究以茉莉叶提取物为原料,通过还原溶胶-凝胶法制备钛酸盐(Fe2TiO5和NiTiO3),合成了多功能材料加银钛酸盐。采用x射线衍射、能量色散x射线光谱、拉曼光谱、布鲁诺尔-埃米特-泰勒比表面积、扫描电子显微镜和紫外-可见吸收光谱对所得材料的物理化学特性进行了测定。结果表明,银在Fe2TiO5和NiTiO3表面分散良好,形成具有两个吸光区的光催化剂。所得材料作为抗菌剂应用于污水处理。Ag-Fe2TiO5 (Ag-FTO)样品比Ag-NiTiO3 (Ag-NTO)样品表现出更好的性能和抗菌活性,这是由于银纳米粒子在FTO表面有更好的分散。此外,与革兰氏阳性(+)细菌相比,抗菌结果对革兰氏阴性(−)细菌的抑制活性增强。成功合成了添加Ag的纳米材料Fe2TiO5和NiTiO3。这些材料对蜡样芽孢杆菌、大肠杆菌、铜绿假单胞菌、伤寒沙门氏菌和金黄色葡萄球菌具有良好的抑制作用。此外,Ag-Fe2TiO5样品的抗菌活性明显优于Ag-NiTiO3样品。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Antibacterial activity of green fabricated silver-doped titanates
Objectives. The study aimed to synthesize the multifunctional materials silver-added titanates via reduction of sol-gel fabricating titanates (Fe2TiO5 and NiTiO3) with Jasminium subtriplinerve Blume leaf extract.Methods. The physicochemical characteristics of the obtained materials were determined by X-ray diffraction, energy dispersive X-Ray spectroscopy, Raman spectroscopy, Brunauer–Emmett–Teller specific surface area, scanning electron microscopy, and UV–Vis absorption spectroscopy.Results. The results demonstrated good dispersion of silver on the surface of Fe2TiO5 and NiTiO3 to create photocatalysts with two light-absorbing regions. The obtained materials were applied as antibacterial agents in polluted water. The Ag–Fe2TiO5 (Ag–FTO) samples showed better properties and antibacterial activity than Ag–NiTiO3 (Ag–NTO) due to the better dispersion of silver nanoparticles on the FTO surface. Besides, the antibacterial results exhibit increased inhibiting activity against gram-negative (−) bacteria as compared with gram-positive (+) bacteria.Conclusions. Nanomaterials Fe2TiO5 and NiTiO3 added Ag were successfully synthesized. These materials showed excellent inhibition against Baccilus cereus, Escherichia coli, Pseudomonas aeruginosa, Salmonella typhi, and Staphylococcus aureus. Additionally, the Ag–Fe2TiO5 samples showed much better antibacterial activity than the Ag–NiTiO3 sample.
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