铂和钼涂层在高温下激光闪光法测量透明玻璃试样热扩散率的适用性

H. Shibata, H. Ohta, Atsushi Suzuki, Y. Waseda
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引用次数: 15

摘要

对于透明材料,如硅酸盐玻璃,基本上需要激光束的吸收层和红外线的发射层,通过激光闪光法与红外线探测器测量热扩散率。通过溅射在圆盘状透明试样的两侧形成厚度为1.0 μm的铂层和厚度为0.7 μm的钼层。然后在高温下测试这种金属涂层。发现铂薄层可以很好地测量温度低于1000 K的硅玻璃的热扩散率。钼涂层还成功地应用于750 ~ 1569 K温度范围内硅酸盐玻璃的热扩散系数的测量,同时考虑了试样内部的辐射传热。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Applicability of Platinum and Molybdenum Coatings for Measuring Thermal Diffusivity of Transparent Glass Specimens by the Laser Flash Method at High Temperatures
For transparent materials such as silicate glasses, an absorber layer of a laser beam and an emitter layer of an infrared ray are essentially required for measuring thermal diffusivity by the laser flash method with an infrared ray detector. Platinum (thickness: 1.0 μm) and molybdenum (thickness: 0.7 μm) thin layers were formed by sputtering on both sides of a transparent specimen with a disk shape. Then such metal coating was tested at elevated temperatures. The platinum thin layer was found to work well to measure thermal diffusivity of silica glass at temperature below 1000 K. The molybdenum coating was also successfully applied to the measurement of thermal diffusivity for silicate glass in the temperature range between 750 and 1569 K with considering radiative heat transfer inside the specimen.
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