用生物测定法筛选隐藻提取物制备纳米铁氧体

Hafza Murtaza, Aasia Sikander, Umema Murtaza, A. Masroor, F. Ghafoor
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引用次数: 1

摘要

摘要研究了隐藻中纳米铁分子的存在。本研究以正己烷、乙酸乙酯、乙醇和水为溶剂,分别制备了各种叶和茎有机提取物。对生物碱、碳水化合物、油、氨基酸等进行了不同的植物化学测试,以确定它们在提取物中的存在。利用紫外分光光度法和高效液相色谱法对样品进行筛选,比较提取液的波长、吸光度和色谱保留时间。结果表明,所有样品中均含有生物碱、碳水化合物和蛋白质。然而,其他化合物随机存在。光谱分析表明,乙酸乙酯提取物峰最高,水提取物峰最低。利用能量色散x射线能谱(EDX)和扫描电子显微镜(SEM)对镍锌纳米铁氧体的表面性能和尺寸进行了表征。结果表明,样品中镍(Ni)和锌(Zn)含量分别为N的4.27⁒、C的6.89⁒和O的35.5⁒,证实了叶和茎中存在纳米铁氧体。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Bioassay Guided Screening of Cryptolepis Extracts for Onward Synthesis of Nano Ferrites
A study was designed to investigate the presence of nanoferrites in Cryptolepis buchanani. In this study, various leaves and stem organic extracts were prepared separately using the solvents viz., n-hexane, ethyl acetate, ethanol and water. Different phytochemical tests for alkaloids, carbohydrates, oils, amino acids and others were performed to determine their presence in the extracts. These plant extracts were used for screening of sample via UV and HPLC techniques to compare the wavelength and absorbance, and retention time on chromatogram by extracts, respectively. The results showed the presence of alkaloids, carbohydrates and proteins in all the samples. However, other compounds were present randomly. Spectroscopy showed highest peaks with ethyl acetate extracts and the lowest with water. The surface properties and size of nickel-zinc nano ferrites were evaluated by Energy-dispersive X-ray spectroscopy (EDX) and Scanning Electron Microscopy (SEM). The former, showed the presence of nickel (Ni) and zinc (Zn) weighing 4.27⁒ of N ,6.89⁒ of C and 35.5⁒ of O in the sample which confirmed the presence of nano ferrites in leaves and stem of C. buchanani.
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