{"title":"在溶胶和凝胶中加入c70","authors":"H. Xia, Q. Nie, Jian-li Zhang, Yuepin Zhang","doi":"10.1081/FST-100102963","DOIUrl":null,"url":null,"abstract":"C70 is incorporated in gel by a sol-gel process with using 3-amino-propyltriethoxysilane (NH2(CH2)3Si(OC2H5)3, APTS) and 3-glycidoxypropltrimethoxysilane (CH2OCHCH2O(CH2)3Si(OCH3)3, GPTMS) as precursors. C70 is firstly mixed with APTS to form C70-NH2(CH2)3Si(OC2H5)3 compound by the reaction between C70 and amino-group of APTS, and then the compound is hybridized with GPTMS to form solid gel. The linkage of C70 and APTS is estimated and confirmed with FT-IR spectra, and the UV/Visible spectra of the sol and gel are measured.","PeriodicalId":12470,"journal":{"name":"Fullerene Science and Technology","volume":"12 1","pages":"161 - 166"},"PeriodicalIF":0.0000,"publicationDate":"2001-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"INCORPORATED C70 IN SOL AND GEL\",\"authors\":\"H. Xia, Q. Nie, Jian-li Zhang, Yuepin Zhang\",\"doi\":\"10.1081/FST-100102963\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"C70 is incorporated in gel by a sol-gel process with using 3-amino-propyltriethoxysilane (NH2(CH2)3Si(OC2H5)3, APTS) and 3-glycidoxypropltrimethoxysilane (CH2OCHCH2O(CH2)3Si(OCH3)3, GPTMS) as precursors. C70 is firstly mixed with APTS to form C70-NH2(CH2)3Si(OC2H5)3 compound by the reaction between C70 and amino-group of APTS, and then the compound is hybridized with GPTMS to form solid gel. The linkage of C70 and APTS is estimated and confirmed with FT-IR spectra, and the UV/Visible spectra of the sol and gel are measured.\",\"PeriodicalId\":12470,\"journal\":{\"name\":\"Fullerene Science and Technology\",\"volume\":\"12 1\",\"pages\":\"161 - 166\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2001-04-15\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Fullerene Science and Technology\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1081/FST-100102963\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Fullerene Science and Technology","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1081/FST-100102963","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
C70 is incorporated in gel by a sol-gel process with using 3-amino-propyltriethoxysilane (NH2(CH2)3Si(OC2H5)3, APTS) and 3-glycidoxypropltrimethoxysilane (CH2OCHCH2O(CH2)3Si(OCH3)3, GPTMS) as precursors. C70 is firstly mixed with APTS to form C70-NH2(CH2)3Si(OC2H5)3 compound by the reaction between C70 and amino-group of APTS, and then the compound is hybridized with GPTMS to form solid gel. The linkage of C70 and APTS is estimated and confirmed with FT-IR spectra, and the UV/Visible spectra of the sol and gel are measured.
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