桃金娘精油的化学成分及理化性质研究

Z. Hagos, Afework Mulugeta, V. Gopalakrishnan, K. Chaithanya, B. Nagaraju
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引用次数: 6

摘要

目的:采用气相色谱-质谱联用技术对桃金娘叶挥发油进行提取,测定其理化性质和化学成分。方法:取500 g粉末状物质(干叶),用clevenger式蒸馏仪加水蒸馏3小时,用无水硫酸钠干燥精油。测定了挥发油的溶解度、密度、比重、折射率、旋光度、比旋光度、酸值、皂化值、酯值等理化性质,用于测定植物叶片精油的质量。采用气相色谱-质谱法对桃金娘叶挥发油的化学成分进行了分析。结果:桃金娘叶精油得率为0.4630.001 g/100 g,提取率为0.4630.001 % (w/w),颜色淡黄色,香气宜人。桃金娘叶精油微溶于水和乙醇,易溶于氯仿、石油醚和乙酸乙酯。经气相色谱-质谱分析,28种成分占总油成分的99.949%。结论:通过对桃金娘叶精油的提取和GC-MS分析,表明桃金娘叶精油具有次生代谢产物的潜力,可作为生物活性物质的良好来源开发利用。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Chemical Composition and Physicochemical Properties of Essential Oil from Myrtus communis
Objective: The objective of the study was to extract the essential oil and to determine the physicochemical properties, chemical composition of the essential oil from Myrtus communis leaves by using GC-MS. Methods: 500 g of the powdered material (dried leaves) was subjected to hydro-distillation using Clevenger-type apparatus for 3 hours and the essential oil was dried over anhydrous sodium sulphate. The physicochemical properties essential oil such as solubility, density, specific gravity, refractive index, optical rotation, specific rotation, acid value, saponification value and ester value were determined, which are used to determine the quality of essential oils extracted from plant leaves. The chemical composition of the essential oil of Myrtus communis leaves was analysed using GC-MS. Results: The yield of essential oil of Myrtus communis leaves was 0.463  0.001 g/100 gram of dry sample which is 0.463  0.001 % (w/w) with pale yellow colour and pleasant odour. The essential oil of Myrtus communis leaves was slightly soluble in water and ethanol while it was soluble in chloroform, petroleum ether and ethyl acetate. The essential oil was subjected to GC-MS analyses, twenty eight components representing 99.949 % of the total oil composition. Conclusion: The present study indicates that the extraction of essential oil from Myrtus communis leaves and GC-MS analysis, the essential oil of this plant have a potential of secondary metabolites which can be exploited as a good source of bioactive substances.
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