田口法合成蜂蜡芯酚醛壳微胶囊

ECSOC-25 Pub Date : 2021-11-13 DOI:10.3390/ecsoc-25-11671
Tejashree Amberkar, P. Mahanwar
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引用次数: 1

摘要

采用田口法考察了间苯二酚改性酚醛壳对蜂蜡微胶囊化工艺参数的影响。采用5 - 3正交试验研究了工艺参数芯壳比、表面活性剂浓度和搅拌速度对控制参数芯含量的影响。核心含量的多少与微胶囊的储热能力成正比。表面活性剂的浓度、芯壳比和搅拌速度分别为3%、1:1和800 rpm。在35 ~ 62℃的温度范围内,以优化的工艺参数值合成的微胶囊形貌为球形,热转变焓为148.93 J/g。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis of Microcapsules with Beeswax Core and Phenol-Formaldehyde Shell by Taguchi Method
: The Taguchi method was used to evaluate effect of process parameters in microencapsulation process of beeswax with resorcinol modified phenol-formaldehyde shell. Orthogonal array of 5 3 was constructed to study effect of process parameters core to shell ratio, surfactant concentration and agitation speed on control parameter core content. The amount of core content is directly proportional to heat storing capacity of microcapsules. Surfactant concentration, core to shell ratio, and agitation speed were optimized at 3%, 1:1, and 800 rpm, respectively. The microcapsules synthesized with optimized process parameters values possessed spherical morphology and heat transition enthalpy 148.93 J/g within temperature range 35 – 62 °C.
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