设计了一种合成2-(1,3-二苯基- 1h -吡唑-4-基)- 1h -苯并咪唑的高效方法

Srinivas B, Prabhakara Rao Koya
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引用次数: 0

摘要

研究了一种简单、高效、环保的合成2-(1,3-二苯基- 1h -吡唑-4-基)- 1h -苯并[d]咪唑的方法,该方法采用三氟甲磺酸钆(III)为催化剂,在乙醇回流反应条件下合成。在优化的反应条件下合成了12个新的2-(1,3-二苯基- 1h -吡唑-4-基)- 1h -苯并咪唑衍生物。这些新产物的结构都得到了光谱分析的证实。该方法操作简单,反应时间短,收率可达85%。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Design an efficient method for the synthesis of 2-(1,3-diphenyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazole
A simple, highly efficient and environmentally friendly method has been developed for the synthesis of 2-(1,3-diphenyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazole by using  Gadolinium(III) trifluoromethanesulfonate catalyst and ethanol reflux reaction conditions  By using this method. 12 new 2-(1,3-diphenyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazole derivatives were synthesized under optimized reactions conditions. All these new products structures are confirmed by spectral analysis. By this method, we achieved imidazole derivatives with more operational simplicity, short reaction time and good yields (up to 85%).  
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