N. Masciocchi, M. Moret, A. Sironi, G. Ardizzoia, S. Cenini, G. L. Monica
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COS trapping by palladium pyrazolates: addition vs. clathration
[{Pd(dmpz)2(Hdmpz)2}2](Hdmpz = 3,5-dimethylpyrazole) reacts with COS, both in solution and in the solid state, affording [Pd{SC(O)dmpz}2] and [{Pd(dmpz)2(Hdmpz)2}2]mdot;COS, respectively; the structure of the latter is determined by ab initio methods from conventional X-ray powder diffraction data only.
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