Ardiansah Ardiansah, Hermin Hardyanti Utami, Shokhul Lutfi, Cherly Firdharini
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引用次数: 0

摘要

血壳废物的好处包括可以用作生物柴油生产的催化剂。本研究的目的是找出血蛤壳制备的催化剂的特性。本研究采用微波和废食用油酯化法和酯交换法。研究结果表明:(1)根据XRD分析结果可知,34.10度角相30的主峰表明所得化合物为氢氧化钙(Ca(OH)2)。2θ角衍射峰位于64.20°,表明存在氧化钙化合物。扫描电镜结果表明,经煅烧后的血蛤壳形状不均匀,部分壳根据Sherrer方程聚集在一起,平均晶粒尺寸为23.77 nm。该工艺制备的生物柴油燃料密度为0.89 g/ml,粘度为4.05 mm /s,酸密度为0.21 Mg KOH/g,总甘油高达0.27%。在油脂和甲醇比为1:12的条件下,以3%wt/wt的浓度,在15分钟内生产生物柴油的最佳质量。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
PreparasiI Katalis Nanomaterial dari Cangkang Kerang Darah (Anadara Granosa Linn) untuk Pembuatan Biodiesel dari Minyak Jelantah dengan Menggunakan Microwave
The benefit of blood shell waste include being used as a catalyst for biodiesel production. This research aims at finding the characteristics of catalysts made of Journal of Chemical Process Engineering e-ISSN Number 2655 2967 9 the blood clamshells. The research applies the methods of esterification and Transesterification by using the microwave and the used cooking oil. The result of the research indicates that (1) based on the XRD analysis results it is known that the main peak of the angle phase of 30 in 34.10 degree shows that the obtained compound is the Hydroxide Calcium (Ca(OH)2) . Besides that the peak of angle diffraction of 2θ on 64.20 ̊ indicates the existence of a calcium oxide compound. The result of SEM points out the shells of the blood clams as the result of calcination have an ununiformed shapes and some of them are aggregated based on the Sherrer equation which produces average crystal sizes of 23.77 nm. The biodiesel fuel produced through the process of blood clamshell catalyst contains the density of 0.89 g/ml, viscosity of 4.05 mm /s, acid density of 0.21 Mg KOH/g and total glycerol as much as 0.27%. The mass with maximum time of biodiesel production is on the minute of 15 with 3%wt/wt of concentration with the oil moll and methanol ration of 1:12.
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