石墨烯-氮化碳纳米结构的一步合成与表征

Khalil Ibrahim Alabid, H. Nasser
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引用次数: 0

摘要

以硫脲为原料,以2.3℃/min的速度在4小时的温度下一步合成了石墨烯-氮化碳。采用傅里叶变换红外光谱(FTIR)、能量色散x射线分析(EDX)、扫描电镜和分光光度法(UV-VIS)对石墨烯-氮化碳进行了表征。石墨烯-氮化碳由三嗪和七嗪结构、碳和氮组成。碳的重量百分比和碳的原子百分比为40.08%,氮的重量百分比和氮的原子百分比为40.08%。因此,通过扫描电镜对石墨烯-氮化碳的比例和尺寸进行了表征,发现其半径在(2µm-147.1 nm)范围内。此外,还发现它在可见光场(VIS)中吸收光。石墨烯-氮化碳的制造和表征的目的是用于制造有机污染物的选择电极(目前用于制造用于分析有机染料的选择电极)。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and Characterization Graphene- Carbon Nitride Nanostructure in One Step
Graphene-carbon nitride can be synthesized from thiourea in a single step at a temperature of four hours at a rate of 2.3 ℃/min. Graphene-carbon nitride was characterized by Fourier-transform infrared spectroscopy (FTIR), energy dispersive X-ray analysis (EDX), scanning electron microscopy, and spectrophotometry (UV-VIS). Graphene-carbon nitride was found to consist of triazine and heptazine structures, carbon, and nitrogen. The weight percentage of carbon and the atomic percentage of carbon are 40.08%, and the weight percentage of nitrogen and the atomic percentage of nitrogen are 40.08%. Therefore, the ratio and the dimensions of the graphene-carbon nitride were characterized by scanning electron microscopy, and it was found that the radius was within the range of (2 µm-147.1 nm). In addition, it was found that it absorbed light in the visible field (VIS). The objective of the manufacture and characterization of graphene-carbon nitride for use in the manufacture of a selective electrode for an organic pollutant (currently used in the manufacture of a selective electrode for the analysis of organic dye).
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