水热法制备微波烧结钛酸锶钡纳米颗粒的表征

S. G. Chavan, A. Tarale, P. M. Kharade, S. Kulkarni, D. J. Salunkhe
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引用次数: 4

摘要

采用水热法合成了钛酸锶钡纳米粒子Ba1−xSrxTiO3 (BSTx),其中x = 0.2和0.3。将BSTx纳米颗粒在800℃下退火1 h以稳定晶相。利用退火后的BSTx在1200℃下微波烧结制备陶瓷体。通过双烧结法有效地合成了BSTx样品。对BST0.20和BST0.30进行了粒度分析、晶体结构分析、介电和铁电性能分析。观察结果很有趣,结果可以与早期的报告相关联和比较。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Characterization of microwave-sintered barium strontium titanate nanoparticles prepared by the hydrothermal method
The hydrothermal technique was used to synthesize barium strontium titanate nanoparticles of Ba1−xSrxTiO3 (BSTx), where x = 0.2 and 0.3. The nanoparticles of BSTx are annealed at 800 °C for 1 h to stabilize the crystalline phase. The annealed BSTx was used to produce ceramic bodies employing a microwave sintering at 1200 °C. Effectively, BSTx samples are synthesized via double-sintering route. BST0.20 and BST0.30 are subjected to the particle size analysis, crystal structure analysis and dielectric and ferroelectric properties. The observations are interesting and the results could be correlated and compared with earlier reports.
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