Saeid Taghavi Fardood, A. Ramazani, Farzaneh Moradnia, Z. Afshari, Sara Ganjkhanlu, F. Zare
{"title":"溶胶-凝胶法绿色合成纳米ZnO及其在微波辐射下无溶剂合成12-芳基四氢苯并[α]杂蒽-11- 1衍生物中的应用研究","authors":"Saeid Taghavi Fardood, A. Ramazani, Farzaneh Moradnia, Z. Afshari, Sara Ganjkhanlu, F. Zare","doi":"10.33945/SAMI/CHEMM.2019.6.2","DOIUrl":null,"url":null,"abstract":"In this work, zinc oxide (ZnO) nanoparticles were fabricated using Arabic gum as a reducing and stabilizing agent by the novel sol-gel method without adding any surfactants. The synthesized nanoparticles were characterized by Fourier transform infrared spectroscopy (FTIR), powder X-ray diffraction (XRD), and scanning electron microscopy (SEM). Subsequently, ZnO nanoparticles as efficient catalysts were consumed for the three-component coupling of 2-naphthol, aldehydes, and dimedone under microwave irradiation and solvent-free conditions in order to furnish the corresponding synthesis of 12-aryl-tetrahydrobenzo[α]xanthene-11-one derivatives in high yields.","PeriodicalId":9896,"journal":{"name":"Chemical Methodologies","volume":"66 1","pages":""},"PeriodicalIF":3.5000,"publicationDate":"2019-08-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"28","resultStr":"{\"title\":\"Green Synthesis of ZnO Nanoparticles via Sol-gel Method and Investigation of Its Application in Solvent-free Synthesis of 12-Aryl-tetrahydrobenzo[α]xanthene-11-one Derivatives Under Microwave Irradiation\",\"authors\":\"Saeid Taghavi Fardood, A. Ramazani, Farzaneh Moradnia, Z. Afshari, Sara Ganjkhanlu, F. Zare\",\"doi\":\"10.33945/SAMI/CHEMM.2019.6.2\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this work, zinc oxide (ZnO) nanoparticles were fabricated using Arabic gum as a reducing and stabilizing agent by the novel sol-gel method without adding any surfactants. The synthesized nanoparticles were characterized by Fourier transform infrared spectroscopy (FTIR), powder X-ray diffraction (XRD), and scanning electron microscopy (SEM). Subsequently, ZnO nanoparticles as efficient catalysts were consumed for the three-component coupling of 2-naphthol, aldehydes, and dimedone under microwave irradiation and solvent-free conditions in order to furnish the corresponding synthesis of 12-aryl-tetrahydrobenzo[α]xanthene-11-one derivatives in high yields.\",\"PeriodicalId\":9896,\"journal\":{\"name\":\"Chemical Methodologies\",\"volume\":\"66 1\",\"pages\":\"\"},\"PeriodicalIF\":3.5000,\"publicationDate\":\"2019-08-20\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"28\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Chemical Methodologies\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.33945/SAMI/CHEMM.2019.6.2\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"CHEMISTRY, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Chemical Methodologies","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.33945/SAMI/CHEMM.2019.6.2","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
Green Synthesis of ZnO Nanoparticles via Sol-gel Method and Investigation of Its Application in Solvent-free Synthesis of 12-Aryl-tetrahydrobenzo[α]xanthene-11-one Derivatives Under Microwave Irradiation
In this work, zinc oxide (ZnO) nanoparticles were fabricated using Arabic gum as a reducing and stabilizing agent by the novel sol-gel method without adding any surfactants. The synthesized nanoparticles were characterized by Fourier transform infrared spectroscopy (FTIR), powder X-ray diffraction (XRD), and scanning electron microscopy (SEM). Subsequently, ZnO nanoparticles as efficient catalysts were consumed for the three-component coupling of 2-naphthol, aldehydes, and dimedone under microwave irradiation and solvent-free conditions in order to furnish the corresponding synthesis of 12-aryl-tetrahydrobenzo[α]xanthene-11-one derivatives in high yields.