1-2二苯乙二氯化铵的合成及晶体结构

Analytical Sciences: X-ray Structure Analysis Online Pub Date : 2008-01-01 DOI:10.2116/ANALSCIX.24.X215

S. Zouari, F. Zouari, N. Chniba-Boudjada, P. Bordet

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引用次数: 0

摘要

1-2二苯乙二氯化铵盐在室温下在极性空间群P21的单斜晶系中结晶;单元胞尺寸为:a = 8.720(2)， b = 6.243(2)， c = 13.972(5) a， β = 106.67(3)°，Z = 2。该结构由[C14H18N2]2+阳离子和分离的氯阴离子组成。这些实体通过N-H…Cl氢键连接在一起，形成一个三维网络。

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Synthesis and Crystal Structure of 1-2 Diphenyl ethylenediammonium Chloride

The salt 1-2 diphenyl ethylenediammonium chloride crystallizes at room temperature in the monoclinic system with polar space group P21; the unit-cell dimensions are: a = 8.720(2), b = 6.243(2), c = 13.972(5)A, β = 106.67(3)° with Z = 2. The structure consists of [C14H18N2]2+ cations and isolated chlorine anions. These entities are linked together through N-H…Cl hydrogen bonds, forming a three-dimentional network.

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Analytical Sciences: X-ray Structure Analysis Online

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