无催化剂、绿色、高效的磁性水中合成1,8-二氧八羟基蒽的方法

Revista de la Sociedad Química de Mexico Pub Date : 2019-12-09 DOI:10.29356/jmcs.v63i4.865

M. Bakherad, Ali Keivanloo, A. Amin, Amir Farkhondeh

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引用次数: 0

摘要

本文报道了以磁化水为绿色溶剂的无催化剂三组分合成1,8-二氧八羟基蒽的方法。醛与1,3-环己二酮/二美酮在磁化水中反应得到9-取代的1,8-二氧基碳羟基蒽衍生物。这种绿色方法具有反应时间短、成本低、后处理程序简单、反应产率定量、不需要有机溶剂等优点。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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Catalyst-free, a Green, and Efficient Protocol for the Synthesis of 1,8-dioxooctahydroxanthenes in Magnetized Water

In this paper, we report the catalyst-free three-component synthesis of 1,8-dioxooctahydroxanthenes in magnetized water as a green solvent. The reaction of aldehydes and 1,3-cyclohexanedione/dimedone in magnetized water gives the 9-substituted 1,8-dioxooctahydroxanthene derivatives. This green method offers the advantages of short reaction times, low-cost, simple work-up procedure, quantitative reaction yields, and no need for an organic solvent.

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Revista de la Sociedad Química de Mexico

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