{"title":"新型[Cu(二胺)(acac)]ClO4混合螯合物的晶体结构","authors":"H. Golchoubian","doi":"10.2116/ANALSCIX.24.X169","DOIUrl":null,"url":null,"abstract":"The title compound was synthesized and characterized by single-crystal X-ray diffraction. This complex was solved in the tetragonal system, space group P41212, with the following unit-cell parameters: a = 13.6010(3)A, c = 13.1885(6)A, Z = 4, V = 2439.70(13)A3. The final R value was R1 = 0.0259 for 27567 measured reflections.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"40 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"7","resultStr":"{\"title\":\"Crystal Structure of a New Mixed-Chelate Complex of [Cu(diamine)(acac)]ClO4\",\"authors\":\"H. Golchoubian\",\"doi\":\"10.2116/ANALSCIX.24.X169\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The title compound was synthesized and characterized by single-crystal X-ray diffraction. This complex was solved in the tetragonal system, space group P41212, with the following unit-cell parameters: a = 13.6010(3)A, c = 13.1885(6)A, Z = 4, V = 2439.70(13)A3. The final R value was R1 = 0.0259 for 27567 measured reflections.\",\"PeriodicalId\":7796,\"journal\":{\"name\":\"Analytical Sciences: X-ray Structure Analysis Online\",\"volume\":\"40 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2008-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"7\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Analytical Sciences: X-ray Structure Analysis Online\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.2116/ANALSCIX.24.X169\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Analytical Sciences: X-ray Structure Analysis Online","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2116/ANALSCIX.24.X169","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 7
摘要
合成了标题化合物，并用单晶x射线衍射对其进行了表征。该配合物在空间群P41212的四边形体系中求解，单元胞参数为:a = 13.6010(3) a, c = 13.1885(6) a, Z = 4, V = 2439.70(13)A3。对于27567个实测反射，最终R值为R1 = 0.0259。
Crystal Structure of a New Mixed-Chelate Complex of [Cu(diamine)(acac)]ClO4
The title compound was synthesized and characterized by single-crystal X-ray diffraction. This complex was solved in the tetragonal system, space group P41212, with the following unit-cell parameters: a = 13.6010(3)A, c = 13.1885(6)A, Z = 4, V = 2439.70(13)A3. The final R value was R1 = 0.0259 for 27567 measured reflections.
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