活性炭/海藻酸盐/纳米纤维素- cu复合材料的合成与表征

Atikah Nur Syahirah, Jasmidi Jasmidi, Z. Muchtar, Siti Rahmah, A. Pulungan, M. Zubir, R. Selly, P. Faradilla
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引用次数: 0

摘要

OPEFB是天然纤维基复合材料的一种来源,具有成为活性炭和纳米纤维素的潜力。本研究旨在合成活性炭/海藻酸盐/纳米纤维素-铜复合材料并对其进行表征。本研究使用的表征是FTIR和PSA。活性炭/海藻酸盐/纳米纤维素- cu复合材料的合成首先采用炭化和H3PO4活化法制备活性炭。然后用NaClO2进行漂白,再用Na2SO3和NaOH进行脱木质素处理,得到纳米纤维素。使用商业海藻酸盐。将三种成分混合均匀后,放入0.1M的CuSO4溶液中制珠。表征结果表明,表征的PSA纳米纤维素粒径为41.05 nm, FTIR表征结果表明,活性炭/海藻酸盐/纳米纤维素- cu复合材料含有官能团OH基团、三C键由拉伸炔、C=C芳香基团、C- h烷烃基团、C-O基团、P=O伸缩振动的P-O-C基团和表达活性炭的醇OH基团;羟基(OH)、羧基、羰基、C-O- c和- cooh键代表海藻酸盐,羟基官能团、伸展的C-H键、伸展的C-O键、伸展的C-C键和葡萄糖单元之间的β-糖苷键表示纳米纤维素。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and Characterization of Activated Carbon/Alginate/Nanocellulose-Cu Composites
OPEFB is one source of natural fiber-based composites which have the potential to become activated carbon and nanocellulose. This study aims to synthesize and characterize the activated carbon/alginate/nanocellulose-Cu composite. The characterization used in this study is FTIR and PSA. The synthesis of activated carbon/alginate/nanocellulose-Cu composites began with a process of carbonization and activation with H3PO4 to produce Activated Carbon. Followed by a bleaching process with NaClO2 and a delignification process with Na2SO3 and NaOH to produce Nanocellulose. Alginate using commercial alginate. Furthermore, the three ingredients were mixed until homogeneous and put into a 0.1M CuSO4 solution to produce beads. The results of the characterization of characterization of PSA Nanocellulose obtained a particle size of 41.05 nm and the result of FTIR characterization on the activated carbon/alginate/nanocellulose-Cu composite contained the functional group OH group, triple C bond from stretching alkyne, C=C aromatic group, C-H alkane group, C-O group, the P=O stretching vibration of the P-O-C group and the alcohol OH group expressing the active carbon; there are functional groups of hydroxyl (OH), carboxyl, carbonyl, and C-O-C and –COOH bonds which represent alginate and there are OH functional groups, stretching C-H bonds, C-O stretching, stretching C-C, and β- glucosidic bonds between glucose units which indicate nanocellulose.
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