溶胶-凝胶法制备纯氧化锌和掺杂铟氧化锌纳米粒子的结构和形态特征

M. Poloju, M. V. Ramana Reddy
{"title":"溶胶-凝胶法制备纯氧化锌和掺杂铟氧化锌纳米粒子的结构和形态特征","authors":"M. Poloju, M. V. Ramana Reddy","doi":"10.1109/ICANMEET.2013.6609269","DOIUrl":null,"url":null,"abstract":"High purity ZnO nano particles and Indium (In) doped Zinc oxide (ZnO) nano particles were synthesized by simple sol-gel technique at low temperature of 70°C. Different compositions of Indium (In) doped zinc oxide with Zn1-xInxO (x=0.01 to 0.08 atomic percent) were prepared by low cost sol-gel technique. The powders were examined for their structural study using XRD. It has been found from diffraction data that the pure and Indium doped powders have formed to be single phase hexagonal wurtzite crystal structure. The microcstrutured parameters such as strain, lattice constant, particle size, dislocation density, bond lengths between Zn and O were calculated. Using the calculated values of particle size from XRD & SEM crystallinity index was estimated. From the observed crystallinity index data of the prepared nano materials it was confirmed that the materials were showing polycrystalline nature.","PeriodicalId":13708,"journal":{"name":"International Conference on Advanced Nanomaterials & Emerging Engineering Technologies","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2013-07-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"2","resultStr":"{\"title\":\"Structural and morphological features of sol-gel processed pure and Indium doped ZnO nanoparticles\",\"authors\":\"M. Poloju, M. V. Ramana Reddy\",\"doi\":\"10.1109/ICANMEET.2013.6609269\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"High purity ZnO nano particles and Indium (In) doped Zinc oxide (ZnO) nano particles were synthesized by simple sol-gel technique at low temperature of 70°C. Different compositions of Indium (In) doped zinc oxide with Zn1-xInxO (x=0.01 to 0.08 atomic percent) were prepared by low cost sol-gel technique. The powders were examined for their structural study using XRD. It has been found from diffraction data that the pure and Indium doped powders have formed to be single phase hexagonal wurtzite crystal structure. The microcstrutured parameters such as strain, lattice constant, particle size, dislocation density, bond lengths between Zn and O were calculated. Using the calculated values of particle size from XRD & SEM crystallinity index was estimated. From the observed crystallinity index data of the prepared nano materials it was confirmed that the materials were showing polycrystalline nature.\",\"PeriodicalId\":13708,\"journal\":{\"name\":\"International Conference on Advanced Nanomaterials & Emerging Engineering Technologies\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2013-07-24\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"2\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Conference on Advanced Nanomaterials & Emerging Engineering Technologies\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1109/ICANMEET.2013.6609269\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Conference on Advanced Nanomaterials & Emerging Engineering Technologies","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/ICANMEET.2013.6609269","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 2

摘要

采用简单的溶胶-凝胶法制备了高纯氧化锌纳米颗粒和掺杂铟氧化锌纳米颗粒,温度为70℃。采用低成本溶胶-凝胶法制备了Zn1-xInxO (x=0.01 ~ 0.08原子百分比)掺杂铟(In)的氧化锌。用XRD对粉末进行了结构分析。从衍射数据发现,纯粉和掺铟粉均形成了单相六方纤锌矿晶体结构。计算了合金的应变、晶格常数、晶粒尺寸、位错密度、Zn和O之间的键长等微观组织参数。利用XRD和SEM计算得到的粒度值对结晶度指数进行了估算。通过观察所得纳米材料的结晶度指数,证实了材料具有多晶性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Structural and morphological features of sol-gel processed pure and Indium doped ZnO nanoparticles
High purity ZnO nano particles and Indium (In) doped Zinc oxide (ZnO) nano particles were synthesized by simple sol-gel technique at low temperature of 70°C. Different compositions of Indium (In) doped zinc oxide with Zn1-xInxO (x=0.01 to 0.08 atomic percent) were prepared by low cost sol-gel technique. The powders were examined for their structural study using XRD. It has been found from diffraction data that the pure and Indium doped powders have formed to be single phase hexagonal wurtzite crystal structure. The microcstrutured parameters such as strain, lattice constant, particle size, dislocation density, bond lengths between Zn and O were calculated. Using the calculated values of particle size from XRD & SEM crystallinity index was estimated. From the observed crystallinity index data of the prepared nano materials it was confirmed that the materials were showing polycrystalline nature.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信