磷酸二肼的Vilsmeier-Haack反应:4-{[(二甲基)氮杂肼氯铵]甲基}氨基-2,3-二氢-3-氧-4 H - 1,2,4,3 -三氮杂磷孔的合成

IF 0.7 4区管理学 Q3 COMMUNICATION

International Journal of Mobile Communications Pub Date : 2013-01-07 DOI:10.5923/J.IJMC.20120205.02

T. Ali, S. M. Abdel‐kariem

引用次数: 0

摘要

介绍了一种合成4-{((二甲基)氮杂酰基氯铵)甲基}氨基-2,3-二氢- 3-o -o - 4h -1,2,4,3-t氮杂磷孔(2)的简便方法。用Vilsmeier-Haack试剂对膦二肼(1)进行处理，直接得到了高收率的标题化合物。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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Vilsmeier-Haack Reaction of Phosphonic Dihydrazide: Synthesis of 4- {[(Dimethyl)azanylidenonium Chloride] Methyl} Amino-2,3-Dihydro-3-Oxo-4 H -1,2,4, 3-Triazaphosphole

A simp le method for the synthesis of 4-{((dimethyl)azanylidenonium ch loride) methyl}amino-2,3-dihydro- 3-o xo -4H-1,2,4,3-t riazaphosphole (2) is described. Treat ment of phosphonic dihydrazide (1 ) with Vilsmeier-Haack reagent led direct ly to the title co mpound in high yield.

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来源期刊

International Journal of Mobile Communications COMMUNICATION-

自引率

12.50%

发文量

期刊介绍： The world of mobile communications is not a trend, but a phenomenon. IJMC, a fully refereed journal, publishes articles that present current practice and theory of mobile communications, mobile technology, and mobile commerce applications. Topics covered include Integrated mobile marketing communications Wireless advertising/CRM Telematics, pervasive computing Incoming/outgoing wireless links Location management Diffusion, security, efficacy, interaction/integration Metric mobile business enterprises PDAs in services delivery M-/u-business models, m-/u-commerce Digital office, groupware, roomware Mobile ad hoc networking, wireless information assurance Nomadic/portable communications Cross-cultural mobile communications Teaching mobile communication applications Mobile/handheld devices in the classroom, tele-learning.