容量法和仪器法测定火药中硝酸甘油含量的比较分析

Magdalena Rakić, Mirjan Krstovic, Slavko Mijatov, M. Dimić, Bojana Z. Fidanovski
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引用次数: 0

摘要

双基火药的主要能量成分是硝化纤维(NC)和硝化甘油(NG)。在双基火药中,NG被用作增塑剂,同时也是一种高能成分。由于NG在火药中的含量对火药的化学和机械性能或/和特性有很大的影响,因此对NG含量的研究具有重要意义。本文的目的是比较高效液相色谱法和经典分析容积法在无烟火药中硝酸甘油的分离定性测定中的分析性能。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Comparative analysis of volumetric and instrumental method for determination of nitroglycerin content in gunpowder
The major energy components of double-based gunpowder are nitrocellulose (NC) and nitroglycerin (NG). In double-based gunpowder NG is used as a plasticizer and, at the same time, as an energetic component. Since the amount of NG in the gunpowder strongly influences and affects its chemical and mechanical properties or/and characteristics, the study of NG content is of great importance. The aim of this paper is to compare the analytical performances of high-performance liquid chromatography (HPLC) and classic analytical volumetric method for the separation and qualitative determination of nitroglycerine in smokeless gunpowder.
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