醋酸钾动态光度法测定头孢曲松的方法的建立与验证

IF 0.4 Q4 CHEMISTRY, ANALYTICAL
M. Blazheyevskiy, Y. Serdiukova, S. Karpova
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引用次数: 0

摘要

建立了用卡罗酸对头孢曲松纯物质进行动力学修饰的分光光度法定量测定头孢曲松纯物质的方法,并进行了验证。提出了头孢曲松与胡萝卜酸钾反应化学转化的方案。新浪潮的出现使开发头孢曲松定量测定的新方法成为可能。得到的准确度和精密度结果如下:RSD = 1.63 ~ 2.25%, δ = 0.33 ~ 0.96%。LOD = 0.1µg/mL, LOQ = 0.33µg/mL。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Development and Validation of a Simple Procedure for the Kinetic Spectrophotometric Quantitative Determination of Ceftriaxone Using Potassium Caroate
A simple procedure for the quantitative determination of the Ceftriaxone pure substance by the spectrophotometric method in its kinetic modification using Caro’s acid has been developed and validated. The scheme of the chemical transformation of Ceftriaxone with the reaction of potassium caroate has been proposed. The appearance of a new wave gives the possibility of developing a new procedure for the quantitative determination of Ceftriaxone. The obtained results of accuracy and precision are as follows: RSD = 1.63-2.25 %, δ = 0.33-0.96 %. LOD = 0.1 µg/mL, LOQ = 0.33 µg/mL.
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来源期刊
French-Ukrainian Journal of Chemistry
French-Ukrainian Journal of Chemistry CHEMISTRY, ANALYTICAL-
自引率
0.00%
发文量
13
审稿时长
4 weeks
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