乳液聚合法制备十二烷基苯磺酸掺杂四苯胺

K. Basavaiah, K. T. Rao, A. Rao
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引用次数: 6

摘要

在这项工作中,我们报道了用胶束辅助法制备十二烷基苯磺酸(DBSA)掺杂的四苯胺,并对其进行了表征。在这里,DBSA作为四苯胺纳米结构的掺杂剂和模板。用x射线衍射图、傅里叶变换红外光谱、紫外可见光谱、扫描电镜和热重法对合成的DBSA掺杂四苯胺进行了表征。发现四苯胺的形态依赖于n -苯基- 1,4 -苯二胺与DBSA的摩尔比。光谱数据表明DBSA掺杂了四苯胺。热重分析表明,DBSA的掺杂提高了四苯胺的热稳定性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and Characterization of Dodecylbenzene Sulfonic Acid doped Tetraaniline via Emulsion Polymerization
In this work, we report preparation and characterization of dodecylbenzene sulfonic acid (DBSA) doped tetraaniline via micelles assisted method using ammonium per sulphate (APS) as an oxidant. Here, DBSA act as dopant as well as template for tetraaniline nanostructures. The synthesized DBSA doped tetraaniline have been well characterized by X-ray diffraction patterns, Fourier transform infrared spectroscopy, UV-Visible spectroscopy, Scanning electron microscopy and thermogravimetry. The morphologies of tetraaniline were found to be dependent on molar ratios of N-phenyl-1, 4-phenylenediamine to DBSA. The spectroscopic data indicated that DBSA doped tetraaniline. Thermogravimetry studies revealed that the DBSA doping improved the thermal stability of tetraaniline.
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来源期刊
E-journal of Chemistry
E-journal of Chemistry CHEMISTRY, MULTIDISCIPLINARY-
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