{"title":"取代2-氨基苯-1′，3′-噻唑合成过乙酰化β- d -葡萄糖吡喃基硫脲","authors":"N. Thanh","doi":"10.1155/2012/615601","DOIUrl":null,"url":null,"abstract":"Some peracetylated glucopyranosyl thioureas containing a heterocyclic ring system, benzo-1,3-thiazole have been prepared by the condensation reaction of tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate and corresponding substituted 2-amino-(6-substituted)benzo-1,3-thiazoles. Investigated heating conditions showed that the solventless microwave-assisted method gave higher yields of these thioureas.","PeriodicalId":11519,"journal":{"name":"E-journal of Chemistry","volume":"9 1","pages":"55-62"},"PeriodicalIF":0.0000,"publicationDate":"2012-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1155/2012/615601","citationCount":"1","resultStr":"{\"title\":\"Synthesis of Peracetylated β-D-Glucopyranosyl Thioureas from Substituted 2-Aminobenzo-1ʹ, 3ʹ-thiazoles\",\"authors\":\"N. Thanh\",\"doi\":\"10.1155/2012/615601\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Some peracetylated glucopyranosyl thioureas containing a heterocyclic ring system, benzo-1,3-thiazole have been prepared by the condensation reaction of tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate and corresponding substituted 2-amino-(6-substituted)benzo-1,3-thiazoles. Investigated heating conditions showed that the solventless microwave-assisted method gave higher yields of these thioureas.\",\"PeriodicalId\":11519,\"journal\":{\"name\":\"E-journal of Chemistry\",\"volume\":\"9 1\",\"pages\":\"55-62\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2012-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1155/2012/615601\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"E-journal of Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1155/2012/615601\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"E-journal of Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1155/2012/615601","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1
摘要
以4 - o-乙酰基-β- d -葡萄糖吡喃基异硫氰酸酯与相应的2-氨基-(6-取代)苯并-1,3-噻唑为缩合反应，制备了含有杂环体系-苯并-1,3-噻唑的过乙酰化葡萄糖吡喃基硫脲。对加热条件的研究表明，无溶剂微波辅助法制备这些硫脲的收率较高。
Synthesis of Peracetylated β-D-Glucopyranosyl Thioureas from Substituted 2-Aminobenzo-1ʹ, 3ʹ-thiazoles
Some peracetylated glucopyranosyl thioureas containing a heterocyclic ring system, benzo-1,3-thiazole have been prepared by the condensation reaction of tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate and corresponding substituted 2-amino-(6-substituted)benzo-1,3-thiazoles. Investigated heating conditions showed that the solventless microwave-assisted method gave higher yields of these thioureas.
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