Cesar Henrique Zanchi, Fabrício Aulo Ogliari, Ricardo Marques e Silva, Rafael Guerra Lund, Heloisa Har Machado, Carlo Prati, Neftalí Lenin Villarreal Carreño, Evandro Piva
{"title":"硅烷浓度对实验微填充复合树脂性能的影响","authors":"Cesar Henrique Zanchi, Fabrício Aulo Ogliari, Ricardo Marques e Silva, Rafael Guerra Lund, Heloisa Har Machado, Carlo Prati, Neftalí Lenin Villarreal Carreño, Evandro Piva","doi":"10.1186/s40563-015-0054-0","DOIUrl":null,"url":null,"abstract":"<p>The aim of present study was evaluate the effect of different percentages of an organo-functionalized silane monomer as adhesion promoter between barium borosilicate glass fillers and (co)monomer blend in experimental dental composite resin. Gamma-methacryloxypropyltrimethoxysilane (γ-MPS) was assessed in an experimental luting cement, at the concentrations of 0, 1, 3, 5, 7 and 10 (wt%). The experimental resin without fillers was used as control group. The \nflexural strength (FS) and elastic modulus (E) were obtained by mini-flexural test and expressed in MPa and GPa, respectively. Water sorption (WS) and solubility (SL) were determined based on ISO standard 4049:2000. Kruskal–Wallis and Student–Newman–Keuls test were used for comparisons of FS, E and WS. The comparisons of SL means were performed using one-way ANOVA and Tukey’s method (α?=?5?%). The treatment with 3?% silane revealed \nstatistically higher FS, while the group treated with 1?% silane showed statistically higher E than 3?% silane (p?<?0.05) and E similar to control. The experimental composite without filler content showed the highest SL (p?<?0.05) while the control composite showed the highest WS (p?<?0.05). Based on present findings, flexural strength and elastic modulus can sometimes be improved with lower concentrations (1–3?%) rather than higher concentrations (5–7?%) of the silane (γ-MPS) used as coupling agent on barium borosilicate glass filler microparticles of the dental composite resin.</p>","PeriodicalId":464,"journal":{"name":"Applied Adhesion Science","volume":"3 1","pages":""},"PeriodicalIF":1.6800,"publicationDate":"2015-12-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1186/s40563-015-0054-0","citationCount":"22","resultStr":"{\"title\":\"Effect of the silane concentration on the selected properties of an experimental microfilled composite resin\",\"authors\":\"Cesar Henrique Zanchi, Fabrício Aulo Ogliari, Ricardo Marques e Silva, Rafael Guerra Lund, Heloisa Har Machado, Carlo Prati, Neftalí Lenin Villarreal Carreño, Evandro Piva\",\"doi\":\"10.1186/s40563-015-0054-0\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>The aim of present study was evaluate the effect of different percentages of an organo-functionalized silane monomer as adhesion promoter between barium borosilicate glass fillers and (co)monomer blend in experimental dental composite resin. Gamma-methacryloxypropyltrimethoxysilane (γ-MPS) was assessed in an experimental luting cement, at the concentrations of 0, 1, 3, 5, 7 and 10 (wt%). The experimental resin without fillers was used as control group. The \\nflexural strength (FS) and elastic modulus (E) were obtained by mini-flexural test and expressed in MPa and GPa, respectively. Water sorption (WS) and solubility (SL) were determined based on ISO standard 4049:2000. Kruskal–Wallis and Student–Newman–Keuls test were used for comparisons of FS, E and WS. The comparisons of SL means were performed using one-way ANOVA and Tukey’s method (α?=?5?%). The treatment with 3?% silane revealed \\nstatistically higher FS, while the group treated with 1?% silane showed statistically higher E than 3?% silane (p?<?0.05) and E similar to control. The experimental composite without filler content showed the highest SL (p?<?0.05) while the control composite showed the highest WS (p?<?0.05). Based on present findings, flexural strength and elastic modulus can sometimes be improved with lower concentrations (1–3?%) rather than higher concentrations (5–7?%) of the silane (γ-MPS) used as coupling agent on barium borosilicate glass filler microparticles of the dental composite resin.</p>\",\"PeriodicalId\":464,\"journal\":{\"name\":\"Applied Adhesion Science\",\"volume\":\"3 1\",\"pages\":\"\"},\"PeriodicalIF\":1.6800,\"publicationDate\":\"2015-12-22\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1186/s40563-015-0054-0\",\"citationCount\":\"22\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Applied Adhesion Science\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://link.springer.com/article/10.1186/s40563-015-0054-0\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"Dentistry\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Applied Adhesion Science","FirstCategoryId":"1085","ListUrlMain":"https://link.springer.com/article/10.1186/s40563-015-0054-0","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"Dentistry","Score":null,"Total":0}
Effect of the silane concentration on the selected properties of an experimental microfilled composite resin
The aim of present study was evaluate the effect of different percentages of an organo-functionalized silane monomer as adhesion promoter between barium borosilicate glass fillers and (co)monomer blend in experimental dental composite resin. Gamma-methacryloxypropyltrimethoxysilane (γ-MPS) was assessed in an experimental luting cement, at the concentrations of 0, 1, 3, 5, 7 and 10 (wt%). The experimental resin without fillers was used as control group. The
flexural strength (FS) and elastic modulus (E) were obtained by mini-flexural test and expressed in MPa and GPa, respectively. Water sorption (WS) and solubility (SL) were determined based on ISO standard 4049:2000. Kruskal–Wallis and Student–Newman–Keuls test were used for comparisons of FS, E and WS. The comparisons of SL means were performed using one-way ANOVA and Tukey’s method (α?=?5?%). The treatment with 3?% silane revealed
statistically higher FS, while the group treated with 1?% silane showed statistically higher E than 3?% silane (p?<?0.05) and E similar to control. The experimental composite without filler content showed the highest SL (p?<?0.05) while the control composite showed the highest WS (p?<?0.05). Based on present findings, flexural strength and elastic modulus can sometimes be improved with lower concentrations (1–3?%) rather than higher concentrations (5–7?%) of the silane (γ-MPS) used as coupling agent on barium borosilicate glass filler microparticles of the dental composite resin.
期刊介绍:
Applied Adhesion Science focuses on practical applications of adhesives, with special emphasis in fields such as oil industry, aerospace and biomedicine. Topics related to the phenomena of adhesion and the application of adhesive materials are welcome, especially in biomedical areas such as adhesive dentistry. Both theoretical and experimental works are considered for publication. Applied Adhesion Science is a peer-reviewed open access journal published under the SpringerOpen brand. The journal''s open access policy offers a fast publication workflow whilst maintaining rigorous peer review process.