小金刚鹦鹉叶片萜类化合物的分离与鉴定。

Doni Prio Atmoko, E. Marliana, Erwin Erwin
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引用次数: 2

摘要

加拿大马卡兰乙酸乙酯部分萜类化合物的分离与鉴定。已经完成。采用重力柱色谱法和梯度洗脱法对乙酸乙酯馏分进行分离。使用薄层色谱法用各种洗脱剂(即Rf值为0的正己烷、氯仿、甲醇、丙酮和乙酸乙酯)测试所获得的分离物的纯度;0.75;0.80;分别为0.87和0.97。成功分离的萜类化合物是质量为0.0119克的白色晶体。紫外分析在l 207.03 nm处产生1个峰。化合物的FT-IR分析表明,官能团为O-H、脂肪族C-H、脂肪族C=C、C-O和C=O。根据紫外光谱和红外光谱的结果,分离的化合物被认为含有萜类化合物。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
ISOLATION AND CHARACTERIZATION OF TERPENOID COMPOUNDS FROM LEAVES OF Macaranga beccariana Merr.
Isolation and characterization of terpenoid compounds from ethyl acetate fraction of Macaranga beccariana Merr. have been done. The separation process at ethyl acetate fraction using gravity column chromatography with gradient elution method. The obtained isolates were tested for purity using thin layer chromatography with various eluents namely n-hexane, chloroform, methanol, acetone and ethyl acetate with Rf values 0; 0.75; 0.80; 0.87 and 0.97 respectively. The terpenoids which were successfully isolated were white crystals with a mass of 0.0119 grams. UV analysis produced 1 peak at l 207.03 nm. Analysis of compounds with FT-IR indicated the functional groups O-H, aliphatic C-H, aliphatic C=C, C-O and C=O. Based on the results of the UV and FT-IR spectrum, the isolate compounds were thought to contain terpenoids.
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