根据提取方法的比较,确定提取物的化学成分

Ismail Marzuki, Melisa Mirsyah, Selfina Gala
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引用次数: 0

摘要

筛选、鉴定和鉴定典型印度尼西亚植物的化学成分对于在化妆品、医药和食品原料的主要来源中发现高潜力的化学成分是很重要的。选择正确的萃取方法和合适的溶剂类型对获得目标化学成分具有决定性作用。本研究的重点是比较浸提法和浸提法在鉴别吉打邦叶(Terminalia Catappa)化学成分中的应用。选取新鲜、清洗、干燥、捣碎的吉打邦叶进行样品制备。提取分两阶段进行,使用两种溶剂,即第一阶段使用乙醇提取。得到稀释的提取物,然后用旋转蒸发器浓缩。第二次萃取以正己烷为溶剂。采用索氏浸渍法提取的提取物有乙醇提取物和正己烷提取物4种。结果表明:采用浸渍法对吉打邦叶的化学成分进行鉴定,其分离效果优于浸渍法。从吉打邦叶乙醇提取物中鉴定出的化学成分有±20种,以脂肪酸类化合物为主。以正己烷为溶剂,采用蒸馏法和浸取法,均鉴定出两组相似度高达90%的化合物,即脂肪酸基团的4种化学成分(十四烷酸、十六烷酸、十八烷酸、十八烷-9,12 -二烯酸)和脂肪族的2种化学成分(甲基环戊烷、四烷己烷)。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Identifikasi Komponen Kimia Ekstrak Daun Ketapang (Terminalia cattapa) Berdasarkan Perbandingan Metode Ekstraksi
Screening, characterization and identification of chemical components of typical Indonesian plants are important for the purpose of finding high potential chemical components in the use of primary sources of cosmetic, medicinal and food ingredients. The selection of the right extraction method and the appropriate type of solvent is very decisive in the acquisition of the target chemical components. The brand of this research focuses on the comparison of extraction between soxhletation and maceration methods in identifying the chemical components of Ketapang leaves (Terminalia Catappa). Sample preparation was carried out by selecting fresh, cleaned, dried and mashed Ketapang leaves. The extraction was carried out in two stages using two types of solvents, namely the first stage of extraction using ethanol. Obtained a dilute extract, then concentrated using a rotary evaporator. The second extraction used n-hexane as solvent. There are 4 kinds of extracts, each ethanol extract and n-hexane extract by applying the soxhletation and maceration method. The results obtained showed that: the application of the maceration method to the identification of chemical components of ketapang leaves gave relatively better separation results than the soxhletation method. The number of chemical components identified from the ethanol extract of ketapang leaves is ± 20 species which are dominated by fatty acid compounds. There are two groups of chemical compounds identified from ketapang leaves using n-hexane as solvent both in the application of soxhletation and maceration methods with high similarity 90%, namely 4 kinds of chemical components of the fatty acid group (tetradecanoic acid, Hexadecanoic, Octadecanoid, Octadeca-9,12 -Dienoite) and 2 kinds of aliphatic components (methyl cyclopentane, Tetraco Hexane)
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