六铁氧体锶-钙钛矿锶光催化剂纳米复合材料的绿色合成与表征

IF 1.8 3区 化学 Q3 CHEMISTRY, INORGANIC & NUCLEAR
Zahra Hajian Karahroudi, K. Hedayati, M. Goodarzi
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引用次数: 26

摘要

摘要本研究采用绿色自燃法制备了SrFe12O19–SrTiO3纳米复合材料。首先,合成了SrFe12O19纳米颗粒作为核,然后制备了SrTiO3纳米颗粒作为壳,用于制备SrFe12O19–SrTiO3复合材料。以柠檬汁为封端剂,采用溶胶-凝胶自燃绿色合成新方法。采用多种技术对制备的SrFe12O19–SrTiO3纳米复合材料的结构、形态和磁性进行了表征。通过X射线衍射(XRD)研究了纳米复合材料的晶体结构。利用扫描电子显微镜(SEM)研究了SrFe12O19–SrTiO3纳米复合材料的形貌。通过能量色散X射线(EDX)分析了材料的元素组成。利用振动样品磁强计(VSM)在室温下对纳米粉末的磁性能和磁滞回线进行了表征。样品的傅立叶变换红外光谱显示了纳米颗粒的分子谱带。此外,还通过在紫外光照射下降解偶氮染料来检验纳米复合材料的光催化行为。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Green synthesis and characterization of hexaferrite strontium-perovskite strontium photocatalyst nanocomposites
Abstract This study presents a preparation of SrFe12O19– SrTiO3 nanocomposite synthesis via the green auto-combustion method. At first, SrFe12O19 nanoparticles were synthesized as a core and then, SrTiO3 nanoparticles were prepared as a shell for it to manufacture SrFe12O19–SrTiO3 nanocomposite. A novel sol-gel auto-combustion green synthesis method has been used with lemon juice as a capping agent. The prepared SrFe12O19–SrTiO3 nanocomposites were characterized by using several techniques to characterize their structural, morphological and magnetic properties. The crystal structures of the nanocomposite were investigated via X-ray diffraction (XRD). The morphology of SrFe12O19– SrTiO3 nanocomposite was studied by using a scanning electron microscope (SEM). The elemental composition of the materials was analyzed by an energy-dispersive X-ray (EDX). Magnetic properties and hysteresis loop of nanopowder were characterized via vibrating sample magnetometer (VSM) in the room temperature. Fourier transform infrared spectroscopy (FTIR) spectra of the samples showed the molecular bands of nanoparticles. Also, the photocatalytic behavior of nanocomposites has been checked by the degradation of azo dyes under irradiation of ultraviolet light.
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来源期刊
Main Group Metal Chemistry
Main Group Metal Chemistry CHEMISTRY, INORGANIC & NUCLEAR-CHEMISTRY, ORGANIC
CiteScore
4.10
自引率
27.80%
发文量
21
审稿时长
4 weeks
期刊介绍: This journal is committed to the publication of short communications, original research, and review articles within the field of main group metal and semi-metal chemistry, Main Group Metal Chemistry is an open-access, peer-reviewed journal that publishes in ongoing way. Papers addressing the theoretical, spectroscopic, mechanistic and synthetic aspects of inorganic, coordination and organometallic main group metal and semi-metal compounds, including zinc, cadmium and mercury are welcome. The journal also publishes studies relating to environmental aspects of these metals, their toxicology, release pathways and fate. Articles on the applications of main group metal chemistry, including in the fields of polymer chemistry, agriculture, electronics and catalysis, are also accepted.
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