用大麻乳和微波法制备金纳米颗粒

IF 2.2 4区 工程技术 Q2 Chemistry
Claure N. Lunardi, Mirella P. F. Barros, Marina L. Rodrigues, Anderson J. Gomes
{"title":"用大麻乳和微波法制备金纳米颗粒","authors":"Claure N. Lunardi,&nbsp;Mirella P. F. Barros,&nbsp;Marina L. Rodrigues,&nbsp;Anderson J. Gomes","doi":"10.1007/s13404-018-0231-6","DOIUrl":null,"url":null,"abstract":"<p>Uniformly sized and shaped gold nanoparticles (AuNP) were produced by microwave irradiation using <i>Euphorbia tirucalli</i> latex. The AuNPs were characterized by ultraviolet visible spectroscopy (UV–Vis), Fourier transform infrared spectroscopy (FTIR), dynamic light scattering, zeta potential, and transmission electron microscopy (TEM). UV–Vis analysis was employed to detect the characteristic surface plasmon resonance pattern of the AuNPs (550?nm). The carboxylic and polyphenolic groups were associated with the euphol-capped AuNP, which was confirmed using FTIR spectroscopy. The AuNPs studied here show a <i>z</i>-average diameter varying from 35 to 500?±?0.8?nm. TEM reveals that the particles were spherical and polydispersed. The latex itself is very toxic and can be harmful during manipulation, thus highlighting a negative aspect in it use. However, we have demonstrated that the isolation procedure did not impair the reduction action of the dry latex powder. This study provides a robust solution for the synthesis of stable capped gold nanoparticles. Furthermore, the dried powdered <i>E. tirucalli</i> latex seems to be an attractive capping agent for nanoparticles in drug delivery.</p>","PeriodicalId":55086,"journal":{"name":"Gold Bulletin","volume":null,"pages":null},"PeriodicalIF":2.2000,"publicationDate":"2018-06-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1007/s13404-018-0231-6","citationCount":"9","resultStr":"{\"title\":\"Synthesis of gold nanoparticles using Euphorbia tirucalli latex and the microwave method\",\"authors\":\"Claure N. Lunardi,&nbsp;Mirella P. F. Barros,&nbsp;Marina L. Rodrigues,&nbsp;Anderson J. Gomes\",\"doi\":\"10.1007/s13404-018-0231-6\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>Uniformly sized and shaped gold nanoparticles (AuNP) were produced by microwave irradiation using <i>Euphorbia tirucalli</i> latex. The AuNPs were characterized by ultraviolet visible spectroscopy (UV–Vis), Fourier transform infrared spectroscopy (FTIR), dynamic light scattering, zeta potential, and transmission electron microscopy (TEM). UV–Vis analysis was employed to detect the characteristic surface plasmon resonance pattern of the AuNPs (550?nm). The carboxylic and polyphenolic groups were associated with the euphol-capped AuNP, which was confirmed using FTIR spectroscopy. The AuNPs studied here show a <i>z</i>-average diameter varying from 35 to 500?±?0.8?nm. TEM reveals that the particles were spherical and polydispersed. The latex itself is very toxic and can be harmful during manipulation, thus highlighting a negative aspect in it use. However, we have demonstrated that the isolation procedure did not impair the reduction action of the dry latex powder. This study provides a robust solution for the synthesis of stable capped gold nanoparticles. Furthermore, the dried powdered <i>E. tirucalli</i> latex seems to be an attractive capping agent for nanoparticles in drug delivery.</p>\",\"PeriodicalId\":55086,\"journal\":{\"name\":\"Gold Bulletin\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":2.2000,\"publicationDate\":\"2018-06-16\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1007/s13404-018-0231-6\",\"citationCount\":\"9\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Gold Bulletin\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://link.springer.com/article/10.1007/s13404-018-0231-6\",\"RegionNum\":4,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"Chemistry\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Gold Bulletin","FirstCategoryId":"5","ListUrlMain":"https://link.springer.com/article/10.1007/s13404-018-0231-6","RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"Chemistry","Score":null,"Total":0}
引用次数: 9

摘要

采用微波辐照法制备了尺寸均匀、形状均匀的金纳米颗粒(AuNP)。通过紫外可见光谱(UV-Vis)、傅里叶变换红外光谱(FTIR)、动态光散射、zeta电位和透射电子显微镜(TEM)对AuNPs进行了表征。采用紫外-可见分析方法检测了550nm纳米AuNPs的表面等离子体共振特征。羧基和多酚基团与euphol-capped AuNP相关,用FTIR光谱证实了这一点。本文研究的aunp的z-平均直径在35 ~ 500±0.8 nm之间变化。透射电镜显示,颗粒呈球形,多分散。乳胶本身是非常有毒的,在操作过程中可能是有害的,因此在使用中突出了一个消极的方面。然而,我们已经证明,分离过程并不影响干燥乳胶粉的还原作用。该研究为合成稳定的包覆金纳米颗粒提供了一个强有力的解决方案。此外,干燥的粉末状乳剂似乎是一种有吸引力的纳米颗粒药物递送封盖剂。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Synthesis of gold nanoparticles using Euphorbia tirucalli latex and the microwave method

Synthesis of gold nanoparticles using Euphorbia tirucalli latex and the microwave method

Uniformly sized and shaped gold nanoparticles (AuNP) were produced by microwave irradiation using Euphorbia tirucalli latex. The AuNPs were characterized by ultraviolet visible spectroscopy (UV–Vis), Fourier transform infrared spectroscopy (FTIR), dynamic light scattering, zeta potential, and transmission electron microscopy (TEM). UV–Vis analysis was employed to detect the characteristic surface plasmon resonance pattern of the AuNPs (550?nm). The carboxylic and polyphenolic groups were associated with the euphol-capped AuNP, which was confirmed using FTIR spectroscopy. The AuNPs studied here show a z-average diameter varying from 35 to 500?±?0.8?nm. TEM reveals that the particles were spherical and polydispersed. The latex itself is very toxic and can be harmful during manipulation, thus highlighting a negative aspect in it use. However, we have demonstrated that the isolation procedure did not impair the reduction action of the dry latex powder. This study provides a robust solution for the synthesis of stable capped gold nanoparticles. Furthermore, the dried powdered E. tirucalli latex seems to be an attractive capping agent for nanoparticles in drug delivery.

求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
Gold Bulletin
Gold Bulletin 工程技术-材料科学:综合
CiteScore
3.30
自引率
4.50%
发文量
0
审稿时长
3 months
期刊介绍: Gold Bulletin is the premier international peer reviewed journal on the latest science, technology and applications of gold. It includes papers on the latest research advances, state-of-the-art reviews, conference reports, book reviews and highlights of patents and scientific literature. Gold Bulletin does not publish manuscripts covering the snthesis of Gold nanoparticles in the presence of plant extracts or other nature-derived extracts. Gold Bulletin has been published over 40 years as a multidisciplinary journal read by chemists, physicists, engineers, metallurgists, materials scientists, biotechnologists, surface scientists, and nanotechnologists amongst others, both within industry and academia. Gold Bulletin is published in Association with the World Gold Council.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信