含（2-（2-吡啶基）苯并咪唑的糖精酸银配合物的合成与表征

IF 0.2 Q4 CHEMISTRY, MULTIDISCIPLINARY

Revista Colombiana de Quimica Pub Date : 2018-05-01 DOI:10.15446/REV.COLOMB.QUIM.V47N2.68225

Mario Ceroni Galloso, J. Angulo-Cornejo, Maria Nieves Lino-Pacaheco, C. Huerta, Enzo Martín Casimiro Soriano

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引用次数: 2

摘要

以糖化银(I)与2-(2-吡啶基)苯并咪唑(pbi)为原料，以64%的收率合成了一种新的银配位化合物Ag(sac)(pbi)。通过元素分析、IR、uv -可见、XPS、1h - nmr和13c - nmr进行表征。根据结果，银通过三个氮原子配位:一个来自糖精，另一个来自2-(2-吡啶基)苯并咪唑，与这个配体形成一个五元螯合环。

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Synthesis and characterization of mixed-ligand silver(I) saccharinate complex containing (2-(2-pyridyl)benzimidazole

A new silver coordination compound [Ag(sac)(pbi)] was synthesized by reaction of silver(I) saccharinate with 2-(2-pyridyl)benzimidazole (pbi) in 64% yield. The characterization was performed by elemental analysis, IR, UV-Visible, XPS, 1 H-NMR, and 13 C-NMR spectroscopy. According to the results, silver is coordinating through three nitrogen atoms: one from saccharinate and the others from 2-(2-pyridyl)benzimidazole forming with this ligand a five-membered chelate ring.

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来源期刊

Revista Colombiana de Quimica CHEMISTRY, MULTIDISCIPLINARY-

CiteScore

1.50

自引率

0.00%

发文量

期刊介绍： The Revista Colombiana de Química - Colombian Journal of Chemistry (Rev. Colomb. Quim.) Is a peer-reviewed scientific journal of the Department of Chemistry, Faculty of Sciences of the Universidad Nacional de Colombia, Bogotá. It currently publishes three volumes per year: January-April, May-August and September-December. All the content published by the Journal (available online) is under a Creative Commons attribution license type BY 4.0, that allows any person or entity in the world to freely access the content, share it, download it, adapt it or make derivative works without any restriction, provided that it adequately indicates the credit to the authors and to the Colombian Journal of Chemistry.