化学法制备氧化锌纳米颗粒的表面表征。

Q3 Materials Science
Soamyaa Srivastava, J. Manjhi
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引用次数: 1

摘要

氧化锌纳米颗粒属于新时代的纳米材料,在生物医学和现代治疗干预方面有着巨大的应用。自那以后,目前的抗菌治疗方法在各个层面上都失败了。因此,最近的研究致力于合成稳定的氧化锌纳米颗粒。因此,探索了氧化锌纳米颗粒作为替代处理方案的应用。在目前的研究中,氧化锌纳米颗粒的制备是通过湿法化学方法进行的。为了进一步证实合成材料的纯度和稳定性,通过ζ电位分析、热重分析、差示扫描量热法、透射电子显微镜和扫描电子显微镜进行了表征。SEM和TEM揭示了氧化锌纳米颗粒的球形结构,在几个点也有轻微的团聚。通过热重分析和差示扫描量热法测试了热稳定性,描绘了纳米材料在非常高的温度下的强度。使用能量分散X射线光谱法评估元素组成,显示96.01%的锌和3.99%的氧,证明了合成的氧化锌纳米颗粒的纯度。它证实,除了锌和氧之外,不存在其他元素。以硝酸锌和氢氧化钠为原料,采用湿法合成了氧化锌纳米粒子。这种制造过程可靠、廉价,并产生最稳定的副产品。通过几种分析技术进行了表征,以检查合成的纳米材料的真实性,从而表明所获得的ZnO纳米颗粒可以作为一种安全的选择用于医疗干预。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Surface Characterization of Zinc Oxide Nanoparticles Synthesized Via Chemical Route.
Zinc oxide nanoparticles belong to the new age nanomaterials, they are being used tremendously for the advancements of biomedicine and modern therapeutic intervensions. Since, the current antimicrobial treatment methods are failing on various levels. Thus, The recent study is dedicated to synthesizing stable zinc oxide nanoparticles . Therefore, the application of zinc oxide nanoparticles as an alternative treatment option is explored. In the current research fabrication of zinc oxide nanoparticlesis carried out via the wet chemical method. To further confirm the purity and stability of the synthesized material, characterization was performed via zeta potential analysis, Thermogravimetric analysis, Differential Scanning calorimetry, Transmission Electron Microscopy and Scanning Electron Microscopy. SEM and TEM revealed the spherical structure of zinc oxide nanoparticles, also having slight agglomeration at a few points. The thermal stability was tested via thermogravimetric analysis and differential Scanning Calorimetry depicting the strength of the nanomaterial at a very high temperature. Elemental composition was evaluated using Energy Dispersive X-ray Spectroscopy showing 96.01% zinc and 3.99% oxygen, demonstrating the purity of the synthesized zinc oxide nanoparticles. It confirms that no other elements are present apart from zinc and oxygen. Zinc oxide nanoparticles were synthesized via wet chemical method using zinc nitrate and sodium hydroxide. This fabrication procedure is reliable, cheap, and yields the most stable by-products. Characterization was carried out via several analytical techniques to check the authenticity of the synthesized nanomaterial, thus revealing that the obtained ZnO nanoparticles could be used in medical interventions as a safe option.
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来源期刊
Current Nanomaterials
Current Nanomaterials Materials Science-Materials Science (miscellaneous)
CiteScore
1.60
自引率
0.00%
发文量
53
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