二羧酸银环己烷的制备:Β-cyclodextrin包合物及其在聚乙烯醇纳米网中的应用

Q4 Engineering

Tekstil ve Muhendis Pub Date : 2020-12-30 DOI:10.7216/1300759920202712002

Rıza Atav, A. Yıldız, Derman Vatansever Bayramol, A. Agirgan, Uğur Ergünay

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引用次数: 2

摘要

本研究采用捏合和物理混合技术制备了环己烷二羧酸银（Ag-CdC）与β-环糊精的主客体包合物，并通过傅立叶变换红外光谱（FTIR）和热重分析仪（TGA）进行了分析。制备了客体与客体1:1和1:2的化学计量。FTIR和TGA结果表明，环己烷二羧酸银（Ag-CdC）：β-环糊精（β-CD）包合物的质量比分别为1:1和1:2。此外，在静电纺丝过程中，将这些制备的包合物掺杂在聚乙烯醇纳米纤维中以获得纳米网。用扫描电子显微镜（SEM）研究了纳米网的形成。此外，还进行了FTIR和TGA分析。结果表明，包合物的制备和包合物添加PVA纳米网的制备都是成功的。

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Preparation of Silver Cyclohexane di Carboxylate: Β-cyclodextrin Inclusion Complexes and Their Use in the Production of Poly(vinyl alcohol) Nanowebs

In this study, guest:host inclusion complexes of silver cyclohexane di carboxylate (Ag-CdC) with β-cyclodextrin were prepared by kneading and physical mixing techniques, and analyzed via Fourier transformed infrared spectroscopy (FTIR) and thermogravimetric analyser (TGA). The 1:1 and 1:2 stoichiometry of the guest:host were prepared. Obtained FTIR and TGA results showed that formation of silver cyclohexane di carboxylate (Ag-CdC): β-cyclodextrin (β-CD) inclusion complexes occurred at a mass ratio of both 1:1 and 1:2. Furthermore, these prepared inclusion complexes were doped in poly(vinyl alcohol) nanofibers during electrospinning process for obtaining nanowebs. The formation of nanowebs were investigated with scanning electron microscopy (SEM). Besides, FTIR and TGA analysis were also carried out. Results showed that both inclusion complex preparation and inclusion complex added PVA nanowebs production were successful.

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来源期刊

Tekstil ve Muhendis Engineering-Industrial and Manufacturing Engineering

CiteScore

0.40

自引率

0.00%

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