基于设计专家的甲基丙烯酸甲酯聚合过程变量优化研究

A. O. Valdivia, C. M. Osorio, Y. V. Rodríguez, Lucila Giammatteo
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引用次数: 1

摘要

聚合物是一系列对食品运输、包装和配送、建筑等许多过程至关重要的材料。因此,了解这一过程所依赖的变量很重要。实验设计是一种强大的工具,可以通过软件构建的实验矩阵来识别对过程有重大影响的变量。为了将信息通信技术应用于某高校聚合物教学过程中,对聚甲基丙烯酸甲酯的聚合过程系统进行了研究。影响珍珠大小的变量是:温度、反应时间和聚乙烯醇水相的体积。这些变量通过Box-Behnken实验设计进行优化,在三个层面上有三个因素,实现了响应面的构建以优化过程,获得了一个三维方程,该方程能够通过自变量的值预测珍珠尺寸。最后,学生获得了操纵影响聚合过程的变量以优化过程的能力。因此,在聚合系统的学习和教学过程中,设计专家是一个有价值的ICT工具。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Variable Optimization in Methylmethacrylate Polymerization by Using Design Expert as a Tool for Implementing ICTs in the Polymeric Systems Learning Process
Polymers constitute a series of materials that are essential for many processes such as: food transport, packaging and distribution, construction, etc. Hence, it is important to understand the variables that this process depends on. Experimental design is a powerful tool that enables the identification of variables that significantly influence a process through a matrix of experiments that a software constructs. With the aim of implementing ICTs in the learning—teaching process of polymers in a university group, the polymerization process system of PPMA (polymethylmethacrylate) is studied. The variables that affect the size of the Pearl are: temperature, reaction time and volumen of the polyvinyl alcohol aqueous phase. These variables are optimized through a Box-Behnken experimental design with three factors in three levels, achieving the construction of the response surface to optimize the process, obtaining a tridimensional equation that enables the prediction of the Pearl size through the values of the independent variables. Finally, the student acquires the competency of manipulating the variables that affect the polymerization process to optimize the process. For this reason, Design Expert is a valuable ICT tool in the learning-teaching process of polymerization systems.
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