{"title":"皂荚提取物对蚕丝的脱胶及响应面法优化","authors":"Harshal Patil, Krupali Surve, Ashok Athalye","doi":"10.1111/cote.12684","DOIUrl":null,"url":null,"abstract":"<p>The present investigation aims to develop a method for degumming Eri silk using <i>Sapindus</i> (soapnut) extract and optimise it using response surface methodology (RSM). The initial experiment was conducted with 10 g/L <i>Sapindus</i> extract for 60 min at a boil, and the initial experiments indicated effective degumming. Further degumming experiments were conducted using RSM to optimise the process parameters, with weight loss being the primary response. The results revealed an optimised recipe for degumming was 9 g/L <i>Sapindus</i> extract at 92°C for 30 min, and the desirability value for this optimised recipe is 0.376. Eri silk that has been alkali-degummed loses more weight than silk degummed with <i>Sapindus</i> extract and soap. Comparatively speaking, degumming with <i>Sapindus</i> extract has a lesser impact on tensile strength than degumming with alkaline and soap. The whiteness, yellowness, brightness, and absorbency values between <i>Sapindus</i> extract and conventional degumming do not significantly differ. Compared with soap and <i>Sapindus</i> extract degumming, alkaline degummed fabric exhibits higher dye uptake. After being degummed with soap and <i>Sapindus</i> extract instead of alkaline, the fabric felt softer. Overall, the results show that both degumming with <i>Sapindus</i> extract and traditional methods are equally effective.</p>","PeriodicalId":10502,"journal":{"name":"Coloration Technology","volume":null,"pages":null},"PeriodicalIF":2.0000,"publicationDate":"2023-02-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Degumming of Eri silk by Sapindus (soapnut) extract and optimisation by response surface methodology\",\"authors\":\"Harshal Patil, Krupali Surve, Ashok Athalye\",\"doi\":\"10.1111/cote.12684\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>The present investigation aims to develop a method for degumming Eri silk using <i>Sapindus</i> (soapnut) extract and optimise it using response surface methodology (RSM). The initial experiment was conducted with 10 g/L <i>Sapindus</i> extract for 60 min at a boil, and the initial experiments indicated effective degumming. Further degumming experiments were conducted using RSM to optimise the process parameters, with weight loss being the primary response. The results revealed an optimised recipe for degumming was 9 g/L <i>Sapindus</i> extract at 92°C for 30 min, and the desirability value for this optimised recipe is 0.376. Eri silk that has been alkali-degummed loses more weight than silk degummed with <i>Sapindus</i> extract and soap. Comparatively speaking, degumming with <i>Sapindus</i> extract has a lesser impact on tensile strength than degumming with alkaline and soap. The whiteness, yellowness, brightness, and absorbency values between <i>Sapindus</i> extract and conventional degumming do not significantly differ. Compared with soap and <i>Sapindus</i> extract degumming, alkaline degummed fabric exhibits higher dye uptake. After being degummed with soap and <i>Sapindus</i> extract instead of alkaline, the fabric felt softer. Overall, the results show that both degumming with <i>Sapindus</i> extract and traditional methods are equally effective.</p>\",\"PeriodicalId\":10502,\"journal\":{\"name\":\"Coloration Technology\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":2.0000,\"publicationDate\":\"2023-02-20\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Coloration Technology\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://onlinelibrary.wiley.com/doi/10.1111/cote.12684\",\"RegionNum\":4,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"CHEMISTRY, APPLIED\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Coloration Technology","FirstCategoryId":"88","ListUrlMain":"https://onlinelibrary.wiley.com/doi/10.1111/cote.12684","RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"CHEMISTRY, APPLIED","Score":null,"Total":0}
Degumming of Eri silk by Sapindus (soapnut) extract and optimisation by response surface methodology
The present investigation aims to develop a method for degumming Eri silk using Sapindus (soapnut) extract and optimise it using response surface methodology (RSM). The initial experiment was conducted with 10 g/L Sapindus extract for 60 min at a boil, and the initial experiments indicated effective degumming. Further degumming experiments were conducted using RSM to optimise the process parameters, with weight loss being the primary response. The results revealed an optimised recipe for degumming was 9 g/L Sapindus extract at 92°C for 30 min, and the desirability value for this optimised recipe is 0.376. Eri silk that has been alkali-degummed loses more weight than silk degummed with Sapindus extract and soap. Comparatively speaking, degumming with Sapindus extract has a lesser impact on tensile strength than degumming with alkaline and soap. The whiteness, yellowness, brightness, and absorbency values between Sapindus extract and conventional degumming do not significantly differ. Compared with soap and Sapindus extract degumming, alkaline degummed fabric exhibits higher dye uptake. After being degummed with soap and Sapindus extract instead of alkaline, the fabric felt softer. Overall, the results show that both degumming with Sapindus extract and traditional methods are equally effective.
期刊介绍:
The primary mission of Coloration Technology is to promote innovation and fundamental understanding in the science and technology of coloured materials by providing a medium for communication of peer-reviewed research papers of the highest quality. It is internationally recognised as a vehicle for the publication of theoretical and technological papers on the subjects allied to all aspects of coloration. Regular sections in the journal include reviews, original research and reports, feature articles, short communications and book reviews.