小型、高温、广角炉，用于广角X射线散射

IF 1.3 4区工程技术 Q4 CHEMISTRY, ANALYTICAL

Instrumentation Science & Technology Pub Date : 2023-03-08 DOI:10.1080/10739149.2023.2186429

Xiaoxia Shang, Weifeng Huang, Yueqian Fan, Haijuan Wu, Meijun Wang, L. Chang, Dongfeng Li, Zhihong Li

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引用次数: 0

摘要

摘要基于同步辐射的广角X射线散射（WAXS）是原位研究高温加热过程中晶体结构变化的理想方法。该贡献描述了一种用于现场WAXS的小型熔炉。该炉具有从0到135°的广泛散射/衍射角，将样品从室温加热到1000 20℃ °C/min，适用于材料的原位WAXS和径向分布函数。提供温度校准和安全验证。通过现场WAXS验证了该炉在烟煤炭化中的应用。

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Small, high temperature, wide-angle furnace for wide-angle X-ray scattering

Abstract Wide-angle X-ray scattering (WAXS) based upon synchrotron radiation is ideal for the in situ study of crystal structural changes during heating at high temperatures. This contribution describes a small furnace for in situ WAXS. The furnace has a wide coverage of scattered/diffracted angle from 0 to 135°, heats samples from room temperature to 1000 °C at 20 °C/min, and is suitable for in situ WAXS and radial distribution function of materials. Temperature calibration and safety verification are provided. The use of the furnace is demonstrated by in situ WAXS for the carbonization of bituminous coal.

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来源期刊

Instrumentation Science & Technology 工程技术-分析化学

CiteScore

3.50

自引率

0.00%

发文量

审稿时长

>12 weeks

期刊介绍： Instrumentation Science & Technology is an internationally acclaimed forum for fast publication of critical, peer reviewed manuscripts dealing with innovative instrument design and applications in chemistry, physics biotechnology and environmental science. Particular attention is given to state-of-the-art developments and their rapid communication to the scientific community. Emphasis is on modern instrumental concepts, though not exclusively, including detectors, sensors, data acquisition and processing, instrument control, chromatography, electrochemistry, spectroscopy of all types, electrophoresis, radiometry, relaxation methods, thermal analysis, physical property measurements, surface physics, membrane technology, microcomputer design, chip-based processes, and more. Readership includes everyone who uses instrumental techniques to conduct their research and development. They are chemists (organic, inorganic, physical, analytical, nuclear, quality control) biochemists, biotechnologists, engineers, and physicists in all of the instrumental disciplines mentioned above, in both the laboratory and chemical production environments. The journal is an important resource of instrument design and applications data.